2,4,6-三甲基苯磺酰肼(16182-15-3)核磁图(¹³CNMR)

Mass

MS-IW-8196          
2,4,6-trimethylbenzenesulfonohydrazide
C9H14N2O2S          (Mass of molecular ion:    214)

   Source Temperature: 150 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      17.0       2.5
      18.0      11.0
      27.0       3.3
      28.0       9.1
      29.0       9.7
      30.0      10.4
      31.0       5.2
      39.0       6.7
      41.0       8.9
      45.0       3.2
      48.0       5.7
      50.0       2.1
      51.0       5.9
      52.0       2.2
      53.0       3.6
      57.5       1.7
      58.0       2.5
      59.0       3.3
      62.0       1.1
      63.0       3.5
      64.0      20.0
      65.0       6.3
      66.0       1.1
      74.0       1.2
      75.0       1.5
      76.0       1.3
      77.0      15.9
      78.0       5.4
      79.0      11.3
      80.0       1.0
      89.0       1.5
      91.0      29.5
      92.0       3.4
      93.0       3.8
     102.0       1.9
     103.0      10.7
     104.0       6.3
     105.0     100.0
     106.0      11.9
     107.0       3.7
     115.0       7.9
     116.0       2.0
     117.0      10.6
     118.0       3.1
     119.0      78.5
     120.0      84.4
     121.0      11.8
     134.0       2.5
     135.0      10.0
     136.0       4.6
     137.0       2.2
     139.0       4.0
     149.0       2.1
     150.0       1.8
     151.0       5.6
     152.0      14.8
     153.0       2.0
     165.0       2.6
     166.0       4.5
     167.0       4.3
     168.0       4.3
     183.0       1.2
     184.0      24.8
     185.0      23.2
     186.0       3.8
     187.0       1.3
     214.0       9.8
     215.0       1.3

Assign. Shift(ppm) A 6.983 B 5.85 C 3.47 D 2.645 E 2.311

     Hz     ppm     Int.

   2791.02   6.984    249
   2790.65   6.983    249
   1388.31   3.474     24
   1057.25   2.646   1000
    923.58   2.311    501