18051-88-2

甲基癸基二氯硅烷(18051-88-2)红外图谱(IR1)

产品名称:甲基癸基二氯硅烷

CAS:18051-88-2

分子式:C11H24Cl2Si

分子量: 255.3

InChI:InChI=1S/C11H24Cl2Si/c1-3-4-5-6-7-8-9-10-11-14(2,12)13/h3-11H2,1-2H3

InChIKey: UFVFNJHZBMHRCO-UHFFFAOYSA-N

Smiles:C(C[Si](Cl)(Cl)C)CCCCCCCC

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-7606          
dichlorodecylmethylsilane
C11H24Cl2Si         (Mass of molecular ion:    254)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       5.5
      28.0       1.0
      29.0      12.2
      36.0       1.6
      39.0       4.4
      41.0      23.9
      42.0       7.7
      43.0      57.7
      44.0       2.0
      53.0       1.4
      54.0       2.5
      55.0      15.6
      56.0      15.2
      57.0      67.3
      58.0       2.9
      63.0       3.9
      65.0       1.5
      67.0       1.7
      68.0       2.1
      69.0      12.7
      70.0      16.1
      71.0      50.6
      72.0       2.8
      78.0       1.7
      79.0       4.6
      81.0       1.7
      82.0       3.4
      83.0       9.7
      84.0      10.3
      85.0      20.8
      86.0       1.4
      93.0       1.4
      96.0       1.7
      97.0       8.3
      98.0       6.1
      99.0       2.9
     101.0       1.0
     105.0       1.6
     107.0       1.0
     111.0       5.8
     112.0       7.2
     113.0     100.0
     114.0       7.4
     115.0      69.6
     116.0       4.3
     117.0      13.2
     119.0       3.2
     121.0       1.2
     127.0       1.1
     133.0       2.1
     140.0      14.9
     141.0      65.3
     142.0       5.7
     143.0      43.8
     144.0       3.6
     145.0       8.1
     147.0       9.2
     148.0       1.3
     149.0       3.2
     154.0       2.5
     155.0      17.9
     156.0       3.5
     157.0      12.1
     158.0       1.5
     159.0       2.3
     161.0       4.6
     163.0       1.7
     167.0       1.2
     169.0       9.5
     170.0       1.3
     171.0       6.0
     173.0       1.1
     183.0       4.1
     185.0       2.7
     197.0       2.8
     199.0       1.8
     211.0       1.6
     213.0       1.1
     218.0       2.8
     219.0       1.2
     220.0       1.1
     225.0       1.1
     239.0       9.8
     240.0       1.6
     241.0       6.7
     242.0       1.1
     243.0       1.3
     254.0       8.6
     255.0       1.5
     256.0       5.8
     257.0       1.0
     258.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₂₄ Cl₂ Si	0.05 ml : 0.5 ml CDCl₃
dichlorodecylmethylsilane

    Assign.     Shift(ppm)

      A             1.50
      B             1.37
      C             1.27
      D             1.107
      E             0.882
      F             0.758

     Hz     ppm     Int.

    607.91   1.522     39
    605.96   1.517     30
    600.34   1.503     66
    599.12   1.500     58
    596.44   1.493     34
    594.73   1.489     43
    592.29   1.483     73
    589.36   1.475     40
    584.59   1.463     32
    583.62   1.461     31
    554.69   1.388     42
    552.61   1.383     38
    547.85   1.371     58
    540.89   1.354     48
    540.65   1.353     48
    536.62   1.343     34
    533.81   1.336     41
    521.12   1.304    108
    507.45   1.270    638
    450.93   1.129    154
    445.56   1.115     60
    442.38   1.107     90
    434.57   1.088    127
    359.62   0.900    118
    352.91   0.884    376
    345.83   0.866    154
    303.22   0.759   1000

in CDCl3