18251-82-6

二异丁胺盐酸盐(18251-82-6)核磁图(¹³CNMR)

产品名称:二异丁胺盐酸盐

CAS:18251-82-6

分子式:C8H20ClN

分子量: 165.7

InChI:InChI=1S/C8H19N.ClH/c1-7(2)5-9-6-8(3)4;/h7-9H,5-6H2,1-4H3;1H

InChIKey: HDSBLUHKYYCLEZ-UHFFFAOYSA-N

Smiles:C(C)(C)CNCC(C)C.Cl

Mass

MS-NW-8244          
diisobutylamine monohydrochloride
C8H19N HCl          (Mass of molecular ion:    129)

   Source Temperature: 200 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      18.0       1.9
      27.0       3.0
      28.0       3.2
      29.0       8.5
      30.0      55.0
      35.0       1.7
      36.0      13.1
      38.0       4.4
      39.0       3.4
      41.0      12.3
      42.0       3.7
      43.0       3.9
      44.0       2.8
      55.0       4.1
      56.0       1.7
      57.0      25.5
      58.0       5.4
      70.0       1.9
      72.0       3.1
      84.0       1.6
      86.0     100.0
      87.0       6.0
     114.0       1.7
     128.0       1.1
     129.0       7.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₉ N	0.044 g : 0.5 ml CDCl₃
diisobutylamine monohydrochloride

    Assign.     Shift(ppm)

      A             9.3
      B             2.81
      C             2.30
      D             1.110

     Hz     ppm     Int.

    262.13   2.927     39
    255.31   2.851     92
    252.63   2.821     27
    249.75   2.789     93
    249.44   2.786     94
    249.00   2.781     93
    243.06   2.714     59
    212.81   2.377     36
    206.25   2.303     43
    199.69   2.230     33
    199.13   2.224     33
    102.38   1.144   1000
     99.38   1.110     49
     98.88   1.105     47
     98.19   1.097     48
     95.81   1.070    837

in CDCl3