4-叔丁基苄溴(18880-00-7)核磁图(¹³CNMR)

Mass

MS-NW-7771          
4-tert-butylbenzyl bromide
C11H15Br            (Mass of molecular ion:    226)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       3.1
      29.0       2.6
      38.0       1.0
      39.0       7.2
      40.0       1.0
      41.0       6.6
      50.0       1.8
      51.0       4.7
      52.0       1.4
      53.0       1.9
      55.0       2.4
      57.0       1.4
      57.5       1.0
      62.0       1.4
      63.0       4.3
      64.0       4.0
      65.0       6.0
      66.0       1.3
      77.0       3.4
      78.0       2.0
      79.0       1.0
      89.0       3.6
      90.0       1.5
      91.0      12.8
      92.0       1.3
     102.0       1.0
     103.0       2.1
     104.0       4.7
     105.0       7.4
     107.0       1.4
     115.0       8.6
     116.0       3.9
     117.0      17.1
     118.0       2.1
     119.0       5.5
     128.0       1.7
     129.0       1.6
     131.0       9.1
     132.0      33.5
     133.0       5.3
     147.0     100.0
     148.0      12.3
     167.0       2.1
     183.0       1.3
     185.0       1.2
     211.0       7.6
     212.0       1.6
     213.0       7.2
     225.0       2.0
     226.0       3.9
     227.0       2.3
     228.0       4.1

Assign. Shift(ppm) A 7.42 B 7.22 C 4.452 D 1.295

     Hz     ppm     Int.

    655.75   7.322    285
    398.81   4.453    210
    116.06   1.296   1000
    114.13   1.275     77