19064-18-7

2,6-二氟苄醇(19064-18-7)核磁图(¹HNMR)

产品名称:2,6-二氟苄醇

CAS:19064-18-7

分子式:C7H6F2O

分子量: 144.12

InChI:InChI=1S/C7H6F2O/c8-6-2-1-3-7(9)5(6)4-10/h1-3,10H,4H2

InChIKey: LVICICZQETYOGS-UHFFFAOYSA-N

Smiles:C1(CO)=C(F)C=CC=C1F

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9448          
2,6-difluorobenzyl alcohol
C7H6F2O             (Mass of molecular ion:    144)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.5
      27.0       1.0
      28.0       3.1
      29.0       7.5
      30.0       2.1
      31.0      13.1
      37.0       2.6
      38.0       3.2
      39.0       4.8
      45.0       1.8
      49.0       2.0
      50.0       9.2
      51.0       9.0
      52.0       1.7
      56.0       2.2
      57.0       9.5
      61.0       3.6
      62.0       6.2
      63.0      17.2
      63.5       1.1
      64.0       1.7
      68.0       5.3
      69.0       5.3
      70.0       4.6
      70.5       1.0
      71.5       6.2
      72.0       1.3
      73.0       1.2
      74.0       5.6
      75.0      35.5
      76.0       4.2
      77.0       8.9
      79.0       1.0
      80.0       1.3
      81.0       5.7
      83.0       1.3
      87.0       1.4
      88.0       3.4
      92.0       1.6
      93.0       3.4
      94.0       6.2
      95.0      62.1
      96.0      20.9
      97.0      12.9
      98.0       1.0
      99.0       1.5
     101.0      10.5
     103.0       1.1
     105.0       2.4
     107.0       6.6
     108.0       1.2
     112.0       1.2
     113.0      10.1
     114.0      11.6
     115.0      42.5
     116.0       4.8
     123.0      76.6
     124.0      21.2
     125.0      11.2
     126.0       5.6
     127.0      55.7
     128.0       4.8
     141.0      10.4
     142.0       1.5
     143.0      75.4
     144.0     100.0
     145.0       7.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₆ F₂ O	0.05 ml : 0.5 ml CDCl₃
2,6-difluorobenzyl alcohol

    Assign.     Shift(ppm)

      A             7.227
      B             6.861
      C             4.711
      D             3.04

     Hz     ppm     Int.

   2903.56   7.266    131
   2897.09   7.250    257
   2895.14   7.245    232
   2890.50   7.233    169
   2888.67   7.229    472
   2886.72   7.224    185
   2882.08   7.212    227
   2880.25   7.207    296
   2873.66   7.191    145
   2756.10   6.897     84
   2754.39   6.893    111
   2749.88   6.881    564
   2746.09   6.872    142
   2741.94   6.861    731
   2737.55   6.850    137
   2733.76   6.841    486
   2729.00   6.829     80
   2727.54   6.825     63
   1882.93   4.712   1000
   1215.58   3.042    158

in CDCl3