3,5-二苯基-1-(4,5-二甲基-2-噻唑基)甲(23305-68-2)核磁图(13CNMR)
分子式:C18H17N5S
分子量: 335.43
InChI:InChI=1S/C18H17N5S/c1-13-14(2)24-18(19-13)23-22-17(15-9-5-3-6-10-15)21-20-16-11-7-4-8-12-16/h3-12,20H,1-2H3
InChIKey: GIFKVQOPAJDJLO-UHFFFAOYSA-N
Smiles:C(=NNC1=CC=CC=C1)(N=NC1=NC(C)=C(C)S1)C1=CC=CC=C1
400 MHz in CDCl3
90 MHz in CDCl3
-
| 1H NMR |
399.65 MHz |
| C18 H17 N5 S
|
0.034 g : 0.5 ml CDCl3
|
| 1-(4,5-dimethyl-2-thiazolyl)-3,5-diphenylformazan
|
 |
Assign. Shift(ppm)
A *1 8.049
B *1 7.654
C *2 7.43
D *2 7.41
E *3 7.348
F *3 7.217
G 5.
J 2.376
|
Hz ppm Int.
3221.44 8.061 79
3219.97 8.057 112
3213.99 8.043 46
3212.77 8.039 101
3211.67 8.037 83
3064.21 7.668 70
3063.11 7.665 90
3056.52 7.648 55
3055.54 7.646 102
3054.57 7.644 91
2975.95 7.447 36
2974.98 7.444 59
2967.65 7.426 165
2966.43 7.423 90
2961.55 7.411 55
2960.08 7.407 164
2953.25 7.390 32
2951.42 7.386 75
2944.09 7.367 30
2942.87 7.364 52
2941.53 7.361 32
2935.42 7.345 59
2890.75 7.234 39
2883.42 7.215 59
949.58 2.377 1000
-
| 1H NMR |
89.56 MHz |
| C18 H17 N5 S
|
0.039 g : 0.5 ml CDCl3
|
| 1-(4,5-dimethyl-2-thiazolyl)-3,5-diphenylformazan
|
|
Assign. Shift(ppm)
A *1 8.05
B *1 7.67
C 7.67
D 7.57 to 6.98
E 2.37
|
Hz ppm Int.
725.38 8.100 80
723.31 8.077 63
722.69 8.070 62
721.13 8.052 50
720.31 8.043 49
719.56 8.035 50
718.88 8.027 47
717.31 8.010 105
715.56 7.990 95
691.31 7.719 60
689.69 7.701 74
684.25 7.641 83
682.69 7.623 136
681.63 7.611 117
671.38 7.497 77
670.69 7.489 83
670.31 7.485 84
669.75 7.479 82
666.38 7.441 130
665.94 7.436 133
663.94 7.414 177
663.25 7.406 182
660.75 7.378 183
658.63 7.355 191
655.75 7.322 122
653.13 7.293 86
651.56 7.276 93
649.81 7.256 77
648.38 7.240 85
647.44 7.230 45
645.31 7.206 59
644.75 7.200 62
212.63 2.375 1000