2338-18-3

2-氨基茚满盐酸盐(2338-18-3)核磁图(¹³CNMR)

产品名称:2-氨基茚满盐酸盐

CAS:2338-18-3

分子式:C9H12ClN

分子量: 169.65128

InChI:InChI=1S/C9H11N.ClH/c10-9-5-7-3-1-2-4-8(7)6-9;/h1-4,9H,5-6,10H2;1H

InChIKey: XEHNLVMHWYPNEQ-UHFFFAOYSA-N

Smiles:C1C2=C(C=CC=C2)CC1N.[H]Cl

Mass

MS-NW-6174          
2-indanamine hydrochloride
C9H11N HCl          (Mass of molecular ion:    133)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      17.0       2.1
      18.0       9.6
      27.0       3.5
      28.0       9.4
      30.0       4.5
      35.0       4.4
      36.0      25.5
      37.0       1.5
      38.0       8.8
      39.0       7.9
      40.0       1.3
      41.0       1.9
      42.0       3.9
      43.0       1.4
      50.0       3.9
      51.0       7.2
      52.0       3.9
      53.0       3.2
      53.5       1.1
      54.0       1.7
      62.0       2.7
      63.0       6.8
      64.0       2.0
      64.5       1.9
      65.0       6.7
      65.5       3.9
      66.0       2.7
      66.5       2.1
      67.0       1.0
      74.0       1.7
      75.0       1.7
      76.0       1.7
      77.0      11.2
      78.0       5.6
      79.0       6.4
      80.0       1.1
      89.0       4.9
      90.0       2.6
      91.0      42.4
      92.0       4.9
     102.0       2.0
     103.0       7.2
     104.0       5.2
     105.0      13.8
     106.0      16.1
     107.0       1.8
     115.0      20.6
     116.0      43.2
     117.0      16.1
     118.0      22.0
     119.0       2.3
     130.0       9.0
     131.0       3.8
     132.0      31.1
     133.0     100.0
     134.0      11.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₉ H₁₁ N	0.040 g : 0.5 ml DMSO-d₆
2-indanamine hydrochloride

    Assign.     Shift(ppm)

      A             8.62
      B             7.264
      C             7.190
      D             3.959
      E     *1      3.259
      F     *1      3.060

     Hz     ppm     Int.

   3446.04   8.623    399
   2911.38   7.285     70
   2908.17   7.277    458
   2904.82   7.269    556
   2902.83   7.264    597
   2899.32   7.255    728
   2895.66   7.246    151
   2881.47   7.210    167
   2877.35   7.200   1000
   2874.15   7.192    593
   2871.86   7.186    613
   2868.65   7.178    629
   2864.69   7.168     63
   1598.97   4.001     34
   1597.44   3.998     34
   1591.64   3.983     89
   1590.12   3.979     80
   1585.85   3.969    147
   1580.05   3.954    151
   1573.94   3.939     95
   1569.06   3.927     36
   1568.60   3.925     36
   1567.99   3.924     37
   1566.93   3.921     38
   1315.77   3.293    382
   1308.14   3.274    380
   1299.44   3.252    561
   1291.66   3.232    517
   1232.91   3.085    541
   1226.81   3.070    519
   1216.43   3.044    366
   1210.48   3.029    357

in DMSO-d6