2524-04-1

二乙基硫代磷酰氯(2524-04-1)核磁图(¹HNMR)

产品名称:二乙基硫代磷酰氯

CAS:2524-04-1

分子式:C4H10ClO2PS

分子量: 188.61

InChI:InChI=1S/C4H10ClO2PS/c1-3-6-8(5,9)7-4-2/h3-4H2,1-2H3

InChIKey: KMJJJTCKNZYTEY-UHFFFAOYSA-N

Smiles:P(Cl)(=S)(OCC)OCC

Mass

MS-NW-2937          
O,O'-diethyl chlorothiophosphate
C4H10ClO2PS         (Mass of molecular ion:    188)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      14.0       1.4
      15.0       7.3
      26.0       6.6
      27.0      44.1
      28.0      16.0
      29.0      70.4
      30.0       1.5
      31.0       2.0
      32.0       3.9
      34.0       1.6
      35.0       1.6
      36.0       2.4
      42.0       1.3
      43.0      11.9
      44.0       2.7
      45.0      64.7
      46.0       1.9
      47.0      17.9
      48.0       2.4
      58.0       1.3
      59.0       2.2
      60.0       9.0
      61.0       5.2
      62.0       1.4
      63.0       5.9
      64.0       1.1
      65.0      17.7
      67.0       2.2
      79.0       7.2
      80.0       5.0
      81.0       1.0
      83.0      18.3
      85.0       5.6
      91.0       1.7
      93.0       3.5
      96.0       5.1
      97.0      76.3
      98.0       1.9
      99.0       9.8
     100.0       6.0
     101.0       2.2
     102.0       1.8
     108.0       1.5
     110.0       1.2
     111.0      15.9
     113.0       5.3
     114.0       2.0
     115.0      28.9
     116.0      62.2
     117.0      13.1
     118.0      22.2
     119.0       1.6
     121.0       1.9
     125.0      24.8
     126.0       1.7
     127.0       4.2
     128.0       1.5
     129.0       1.5
     131.0       2.4
     132.0      71.5
     133.0      40.7
     134.0      26.7
     135.0      14.8
     136.0       1.3
     143.0       8.7
     144.0      64.7
     145.0       8.2
     146.0      24.2
     147.0       2.0
     148.0       1.1
     153.0      10.8
     159.0       2.2
     160.0       7.7
     161.0      16.1
     162.0       3.3
     163.0       5.5
     188.0     100.0
     189.0       5.9
     190.0      36.1
     191.0       1.9
     192.0       1.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₄ H₁₀ Cl O₂ P S	0.05 ml : 0.5 ml CDCl₃
O,O'-diethyl chlorothiophosphate

    Assign.     Shift(ppm)

      A             4.300
      B             1.414
     
     J(P-31,H(B))=1.0HZ
     J(P-31,H(A))=11.0HZ

     Hz     ppm     Int.

    401.69   4.486     71
    400.56   4.473     77
    394.44   4.405    222
    393.50   4.394    235
    390.69   4.363     87
    390.00   4.355     93
    387.25   4.324    251
    386.50   4.316    249
    383.44   4.282    284
    382.94   4.276    266
    380.13   4.245    107
    379.63   4.239    109
    376.19   4.201    354
    369.13   4.122    173
    133.94   1.496    491
    132.94   1.485    510
    129.13   1.442     30
    126.94   1.418    973
    125.94   1.407   1000
    119.75   1.338    436
    118.81   1.327    445

in CDCl3

liquid film

更多供应商

二乙基硫代磷酰氯(2524-04-1)核磁图(1HNMR)

二乙基硫代磷酰氯(2524-04-1)核磁图(¹HNMR)