氯乙酸乙烯酯(2549-51-1)核磁图(¹³CNMR)

Mass

MS-NW-5075          
vinyl chloroacetate
C4H5ClO2            (Mass of molecular ion:    120)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      13.0       1.2
      14.0       5.5
      15.0       8.2
      26.0       3.7
      27.0      22.5
      28.0       2.8
      29.0       5.1
      31.0       2.9
      36.0       1.7
      41.0       1.6
      42.0      17.5
      43.0       5.7
      44.0       9.0
      47.0       1.1
      48.0       2.7
      49.0      48.0
      50.0       1.7
      51.0      15.7
      55.0       1.2
      57.0      20.4
      71.0       2.7
      76.0      10.6
      77.0     100.0
      78.0       6.0
      79.0      32.9
      92.0       2.6
     120.0      10.9
     122.0       3.7

Parameter ppm Hz D(A) 4.996 D(B) 4.700 D(C) 7.266 J(A,B) 1.99 J(A,C) 13.83 J(B,C) 6.24 D(D) 4.150

     Hz     ppm     Int.

   2189.91   7.300    244
   2183.69   7.279    249
   2176.09   7.254    255
   2169.89   7.233    258
   1506.64   5.022    259
   1504.70   5.016    270
   1492.81   4.976    249
   1490.87   4.970    259
   1414.10   4.714    268
   1412.13   4.707    258
   1407.85   4.693    265
   1405.88   4.686    253
   1245.00   4.150   1000