332-14-9

N-苯乙基哌啶(332-14-9)核磁图(¹HNMR)

产品名称:N-苯乙基哌啶

CAS:332-14-9

分子式:C13H19N

分子量: 189.3

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-0866          
1-phenethylpiperidine
C13H19N             (Mass of molecular ion:    189)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      30.0       1.0
      41.0       3.5
      42.0       3.7
      44.0       2.6
      55.0       4.2
      69.0       2.0
      70.0       2.6
      77.0       1.3
      79.0       1.0
      96.0       2.0
      98.0     100.0
      99.0       7.1
     104.0       1.2
     105.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₉ N	0.05 ml : 0.5 ml CDCl₃
1-phenethylpiperidine

    Assign.     Shift(ppm)

      A             7.248
      B             7.18
      C             7.16
      D             2.798
      E             2.542
      F             2.45
      G             1.608
      J             1.439

     Hz     ppm     Int.

   2906.74   7.274    239
   2905.76   7.271    379
   2904.17   7.267    157
   2899.17   7.255    645
   2898.44   7.253    777
   2897.46   7.250    582
   2895.02   7.244    247
   2893.19   7.240    299
   2891.24   7.235    835
   2886.47   7.223     41
   2886.23   7.222     41
   2875.00   7.194    600
   2873.66   7.191    991
   2873.29   7.190   1000
   2871.09   7.185    271
   2869.63   7.181    395
   2867.80   7.176    455
   2866.58   7.173    652
   2865.97   7.172    552
   2863.40   7.165    263
   2861.33   7.160    480
   2859.01   7.154    142
   2855.59   7.146    124
   2854.13   7.142    191
   2852.78   7.139    104
   1127.20   2.821    467
   1121.58   2.807    315
   1119.14   2.801    458
   1115.36   2.791    322
   1110.47   2.779    624
   1023.93   2.563    834
   1019.17   2.551    395
   1018.55   2.549    414
   1015.63   2.542    549
   1014.65   2.539    526
   1012.70   2.534    403
   1007.20   2.521    588
    978.52   2.449    491
    654.91   1.639    281
    649.29   1.625    648
    643.43   1.610    912
    637.82   1.596    811
    632.32   1.583    357
    586.18   1.467    130
    579.96   1.452    275
    574.58   1.438    327
    568.85   1.424    193
    563.35   1.410     79

in CDCl3