羟苯基丙酸N-羟基琥珀酰亚胺酯(34071-95-9)核磁图(1HNMR)
分子式:C13H13NO5
分子量: 263.25
InChI:InChI=1S/C13H13NO5/c15-10-4-1-9(2-5-10)3-8-13(18)19-14-11(16)6-7-12(14)17/h1-2,4-5,15H,3,6-8H2
InChIKey: KYRUKRFVOACELK-UHFFFAOYSA-N
Smiles:C1(CCC(ON2C(=O)CCC2=O)=O)=CC=C(O)C=C1
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Mass
MS-NW-5474
N-(3-(p-hydroxyphenyl)propionyloxy)succinimide
C13H13NO5 (Mass of molecular ion: 263)
Source Temperature: 180 °C
Sample Temperature: 100 °C
Direct, 75 eV
14.0 1.5
15.0 1.7
26.0 6.1
27.0 15.8
28.0 23.6
29.0 6.1
30.0 1.9
31.0 3.3
38.0 1.5
39.0 7.5
40.0 1.3
41.0 1.9
42.0 7.7
43.0 6.4
44.0 1.8
45.0 6.4
50.0 1.7
51.0 4.3
52.0 1.9
53.0 2.7
54.0 1.0
55.0 28.4
56.0 5.8
57.0 2.2
59.0 4.7
62.0 1.2
63.0 2.9
65.0 5.2
66.0 1.1
70.0 2.6
73.0 3.0
74.0 5.3
77.0 12.3
78.0 2.8
79.0 1.7
87.0 12.0
91.0 5.7
94.0 2.1
100.0 1.9
101.0 1.1
103.0 1.5
107.0 100.0
108.0 7.4
115.0 16.1
119.0 2.4
120.0 7.5
121.0 2.0
123.0 1.2
166.0 26.4
167.0 2.6
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C13 H13 N O5
|
0.015 g : 0.5 ml CDCl3
|
| N-(3-(p-hydroxyphenyl)propionyloxy)succinimide
|
 |
Assign. Shift(ppm)
A 7.06
B 6.77
C 5.
D 3.00 to 2.86
E 2.828
|
Hz ppm Int.
638.25 7.127 116
636.88 7.112 61
636.25 7.105 59
631.88 7.056 62
629.56 7.030 213
609.81 6.809 254
607.94 6.789 97
607.63 6.785 98
603.31 6.737 62
601.13 6.713 141
265.88 2.969 103
265.56 2.966 103
261.81 2.924 234
260.19 2.906 256
257.63 2.877 120
256.50 2.865 184
253.38 2.830 1000
250.44 2.797 105
249.75 2.789 99
249.19 2.783 102
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| 1H NMR |
399.65 MHz |
| C13 H13 N O5
|
saturated in CDCl3
|
| N-(3-(p-hydroxyphenyl)propionyloxy)succinimide
|
|
Assign. Shift(ppm)
A 7.078
B 6.771
C 5.4
D 2.97
E 2.86
F 2.84
|
Hz ppm Int.
2843.75 7.116 31
2843.14 7.115 33
2841.43 7.110 40
2840.45 7.108 44
2839.60 7.106 46
2838.75 7.104 53
2832.89 7.089 630
2824.46 7.068 714
2817.63 7.051 35
2817.38 7.050 35
2816.28 7.047 32
2719.60 6.805 30
2717.90 6.801 41
2716.80 6.798 48
2716.31 6.797 51
2715.94 6.796 53
2713.01 6.789 158
2710.21 6.782 841
2708.13 6.777 342
2705.69 6.771 120
2703.61 6.765 307
2701.66 6.761 752
2698.85 6.754 131
2695.56 6.745 40
1211.43 3.032 30
1210.57 3.030 32
1210.21 3.029 33
1209.84 3.028 33
1209.23 3.026 34
1208.62 3.025 35
1207.52 3.022 35
1206.79 3.020 36
1206.42 3.019 39
1206.05 3.018 38
1205.32 3.016 41
1204.71 3.015 40
1204.10 3.013 41
1203.49 3.012 47
1203.25 3.011 47
1201.90 3.008 55
1201.54 3.007 56
1200.93 3.005 62
1195.80 2.993 235
1188.84 2.975 491
1180.79 2.955 463
1177.00 2.946 70
1175.90 2.943 59
1175.29 2.941 55
1174.93 2.940 54
1174.32 2.939 55
1173.46 2.937 63
1173.10 2.936 64
1171.88 2.933 58
1171.39 2.932 60
1171.14 2.931 60
1170.78 2.930 61
1170.17 2.928 63
1169.68 2.927 60
1169.31 2.926 58
1168.58 2.925 56
1167.85 2.923 56
1167.48 2.922 55
1166.99 2.921 56
1166.50 2.919 58
1164.67 2.915 65
1163.94 2.913 72
1163.45 2.912 77
1162.96 2.910 81
1160.40 2.904 112
1159.55 2.902 107
1158.69 2.900 109
1158.08 2.898 108
1157.71 2.897 108
1150.88 2.880 590
1150.51 2.879 590
1146.48 2.869 306
1146.12 2.868 306
1144.29 2.864 537
1142.94 2.860 753
1134.52 2.839 1000
1123.05 2.811 163
1122.19 2.808 156
1121.83 2.808 153
1121.22 2.806 154
1116.82 2.795 60
1115.97 2.793 54
1114.75 2.790 48
1114.14 2.788 42
1113.77 2.787 42
1113.28 2.786 41
1112.43 2.784 37
1111.82 2.782 35
1111.45 2.782 35
1110.96 2.780 33
1110.60 2.779 30
1110.11 2.778 33