3634-67-1

氯三己基硅烷(3634-67-1)核磁图(¹HNMR)

产品名称:氯三己基硅烷

CAS:3634-67-1

分子式:C18H39ClSi

分子量: 319.04

Mass

MS-NW-7618          
chlorotrihexylsilane
C18H39ClSi          (Mass of molecular ion:    318)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       3.5
      28.0       1.9
      29.0       5.9
      39.0       1.8
      41.0       8.7
      42.0       2.0
      43.0       9.3
      55.0       6.5
      56.0       2.0
      57.0       1.6
      59.0       1.3
      63.0       5.8
      65.0       5.6
      67.0       1.4
      69.0       3.4
      71.0       1.1
      78.0       1.8
      79.0      11.2
      80.0       1.3
      81.0       4.2
      83.0       8.7
      84.0       1.3
      85.0       2.2
      91.0       5.0
      92.0       2.8
      93.0      21.5
      94.0       2.4
      95.0       7.3
      97.0       3.2
     105.0       4.5
     106.0       1.6
     107.0      29.6
     108.0       2.9
     109.0      10.6
     111.0       1.4
     113.0       1.9
     117.0       1.5
     119.0      10.8
     120.0       2.5
     121.0       8.2
     122.0       1.4
     123.0       1.8
     131.0       1.8
     133.0       3.5
     134.0       1.1
     135.0       1.6
     147.0       4.3
     148.0       1.2
     149.0      74.7
     150.0       9.2
     151.0      26.9
     152.0       3.2
     153.0       1.0
     163.0       2.0
     177.0       1.6
     191.0       1.2
     199.0       1.3
     205.0       1.0
     215.0       1.6
     217.0       1.3
     233.0     100.0
     234.0      18.7
     235.0      37.3
     236.0       6.7
     237.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₈ H₃₉ Cl Si	0.05 ml : 0.5 ml CDCl₃
chlorotrihexylsilane

    Assign.     Shift(ppm)

      A             1.34
      B             1.29
      C             0.887
      D             0.792

     Hz     ppm     Int.

    571.29   1.430     38
    568.60   1.423     45
    562.74   1.409     96
    561.28   1.405     94
    556.40   1.393    154
    555.30   1.390    149
    554.20   1.387    148
    547.36   1.370    195
    544.92   1.364    215
    543.58   1.361    230
    540.65   1.353    264
    534.18   1.337    228
    532.59   1.333    212
    529.91   1.326    224
    525.39   1.315    262
    524.05   1.312    279
    522.22   1.307    266
    517.82   1.296    399
    515.26   1.290    582
    512.94   1.284    481
    508.91   1.274    383
    361.69   0.906    349
    354.86   0.888   1000
    347.90   0.871    436
    334.23   0.837     34
    325.44   0.815    283
    318.12   0.796    217
    315.80   0.791    171
    314.58   0.788    155
    309.33   0.775    313

in CDCl3