5-甲基-2-硝基茴香醚(38512-82-2)核磁图(¹³CNMR)

Mass

MS-NW-8941          
5-methyl-2-nitroanisole
C8H9NO3             (Mass of molecular ion:    167)

   Source Temperature: 250 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      18.0       1.0
      27.0       3.2
      28.0       3.3
      30.0       2.7
      31.0       1.6
      38.0       2.3
      39.0      15.6
      40.0       2.7
      41.0       4.7
      42.0       1.0
      43.0       2.4
      50.0       7.1
      51.0      16.6
      52.0      13.6
      53.0       6.5
      55.0       1.6
      62.0       3.1
      63.0      10.2
      64.0       3.7
      65.0      44.2
      66.0      11.3
      67.0       1.6
      74.0       1.5
      75.0       1.6
      76.0       2.8
      77.0      28.6
      78.0      28.2
      79.0      10.2
      80.0       1.3
      81.0       3.4
      89.0       9.4
      90.0       4.9
      91.0      64.3
      92.0      23.3
      93.0       6.8
      94.0       6.7
     105.0      20.0
     106.0      18.8
     107.0      11.8
     108.0       1.5
     109.0       9.5
     110.0       1.1
     119.0       1.8
     120.0     100.0
     121.0       8.3
     122.0       2.4
     137.0      32.0
     138.0       6.2
     150.0       1.1
     167.0      82.8
     168.0       8.0

Assign. Shift(ppm) A 7.780 B 6.87 C 6.82 D 3.944 E 2.419

     Hz     ppm     Int.

    701.31   7.831     97
    693.25   7.741    118
    615.19   6.870    172
    612.81   6.843     47
    607.00   6.778     62
    606.38   6.771     65
    605.38   6.760     53
    604.75   6.753     44
    353.25   3.945   1000
    216.75   2.421    590