392-69-8

2,4,6-三甲基氟苯(392-69-8)核磁图(¹HNMR)

产品名称:2,4,6-三甲基氟苯

CAS:392-69-8

分子式:C9H11F

分子量: 138.18

InChI:InChI=1S/C9H11F/c1-6-4-7(2)9(10)8(3)5-6/h4-5H,1-3H3

InChIKey: ZLGPNBBJPOBSLY-UHFFFAOYSA-N

Smiles:C1(C)=CC(C)=CC(C)=C1F

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-8198          
2-fluoro-1,3,5-trimethylbenzene
C9H11F              (Mass of molecular ion:    138)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       1.1
      39.0       2.4
      41.0       1.0
      50.0       1.0
      51.0       3.0
      57.0       2.0
      63.0       1.6
      65.0       1.2
      68.0       1.8
      75.0       1.6
      77.0       4.5
      83.0       2.1
      91.0       2.5
      95.0       1.4
      96.0       2.3
      97.0       2.2
     101.0       2.6
     102.0       1.0
     103.0       5.1
     109.0       5.4
     115.0       3.9
     121.0       2.3
     122.0       2.5
     123.0     100.0
     124.0       9.1
     133.0       1.9
     135.0       2.2
     136.0       1.2
     137.0      21.3
     138.0      59.9
     139.0       5.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₁ F	0.05 ml : 0.5 ml CDCl₃
2-fluoro-1,3,5-trimethylbenzene

    Assign.     Shift(ppm)

      A             6.747
      B             2.196
      C             2.185

     Hz     ppm     Int.

   2700.44   6.758    184
   2699.83   6.756    194
   2693.48   6.740    191
   2692.87   6.739    201
    880.62   2.204    549
    875.37   2.191    760
    873.17   2.185   1000

in CDCl3