对甲基苯磺酰氟(455-16-3)核磁图(¹³CNMR)

Mass

MS-NW-6714          
p-toluenesulfonyl fluoride
C7H7FO2S            (Mass of molecular ion:    174)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       2.0
      28.0       1.3
      38.0       2.5
      39.0      14.6
      40.0       1.2
      41.0       3.3
      50.0       5.3
      51.0       7.0
      52.0       2.2
      53.0       1.5
      61.0       1.6
      62.0       4.3
      63.0      11.2
      64.0       3.1
      65.0      25.1
      66.0       1.5
      67.0       1.0
      74.0       1.4
      75.0       1.3
      77.0       9.2
      78.0       3.5
      79.0       7.6
      86.0       1.1
      89.0      10.3
      90.0       8.1
      91.0     100.0
      92.0       7.9
     106.0       1.7
     107.0       8.0
     109.0       2.6
     173.0       1.1
     174.0      57.1
     175.0       5.0
     176.0       3.2

Assign. Shift(ppm) A 7.879 B 7.422 C 2.487

     Hz     ppm     Int.

    712.50   7.956     36
    710.63   7.935    305
    708.94   7.916    114
    704.06   7.862    115
    702.19   7.841    466
    700.63   7.824     81
    670.81   7.491     36
    669.00   7.470    222
    668.06   7.460    315
    667.38   7.452    290
    662.25   7.395     53
    660.31   7.373    201
    659.63   7.366    214
    658.69   7.355    150
    223.06   2.491    990
    222.69   2.487   1000