4925-71-7

CIS-9-OXABICYCLO[6.1.0]NONANE(4925-71-7)核磁图(¹HNMR)

产品名称:CIS-9-OXABICYCLO[6.1.0]NONANE

CAS:4925-71-7

分子式:C8H14O

分子量: 126.2

InChI:InChI=1/C8H14O/c1-2-4-6-8-7(9-8)5-3-1/h7-8H,1-6H2/t7-,8+

InChIKey: MELPJGOMEMRMPL-OCAPTIKFNA-N

Smiles:[C@@]12([H])[C@@]([H])(O1)CCCCCC2 |&1:0,2,r|

Mass

MS-NW-8689          
cis-9-oxabicyclo(6.1.0)nonane
C8H14O              (Mass of molecular ion:    126)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.0
      26.0       1.2
      27.0      18.3
      28.0       5.1
      29.0      21.2
      31.0       1.8
      38.0       1.0
      39.0      21.5
      40.0       3.7
      41.0      68.8
      42.0      26.6
      43.0      16.8
      44.0       4.8
      45.0       1.3
      51.0       1.6
      53.0       6.7
      54.0      34.1
      55.0     100.0
      56.0      25.9
      57.0      44.4
      58.0       7.3
      59.0       2.0
      65.0       1.7
      66.0       1.8
      67.0      53.2
      68.0       9.3
      69.0      16.9
      70.0      14.2
      71.0       9.1
      72.0      11.2
      77.0       1.6
      79.0       7.6
      80.0       5.1
      81.0       7.5
      82.0      13.8
      83.0      28.3
      84.0      13.5
      85.0       3.1
      91.0       1.0
      93.0       5.9
      95.0       2.2
      97.0      19.2
      98.0      14.8
      99.0       1.5
     111.0       6.3
     126.0       2.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₄ O	0.043 g : 0.5 ml CDCl₃
cis-9-oxabicyclo[6.1.0]nonane

    Assign.     Shift(ppm)

      A             2.89
      B     *1      2.13
      C     *1   1.88 to 0.95

     Hz     ppm     Int.

    268.63   3.000     71
    266.25   2.973    131
    264.50   2.954    218
    256.88   2.869    267
    254.06   2.837    214
    197.50   2.206    182
    187.00   2.088    165
    157.38   1.758     58
    136.56   1.525    862
    134.06   1.497   1000
    108.13   1.208     96
     98.81   1.104     33
     97.25   1.086     34

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

更多供应商

CIS-9-OXABICYCLO[6.1.0]NONANE(4925-71-7)核磁图(1HNMR)

CIS-9-OXABICYCLO[6.1.0]NONANE(4925-71-7)核磁图(¹HNMR)