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返回ChemicalBook首页>CAS数据库列表>55770-03-1更多图谱> Α-(氰基亚氨基)-3,4-二氯苯乙胺(55770-03-1)核磁图(13CNMR)

55770-03-1

Α-(氰基亚氨基)-3,4-二氯苯乙胺(55770-03-1)核磁图(13CNMR)

分子式:C9H7Cl2N3

分子量: 228.08

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    Mass

    MS-NW-9999          
    alpha-cyanoimino-3,4-dichlorophenethylamine
    C9H7Cl2N3           (Mass of molecular ion:    227)
    

       Source Temperature: 200 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          18.0       4.2
          27.0       1.3
          28.0       5.3
          36.0       2.4
          37.0       1.3
          38.0       2.0
          39.0       4.6
          41.0       3.1
          42.0      23.6
          43.0      20.8
          44.0       1.3
          49.0       1.3
          50.0       3.6
          51.0       2.3
          56.5       1.2
          57.5       1.8
          61.0       3.2
          61.5       1.4
          62.0       5.8
          63.0      10.1
          64.0       1.8
          68.0      34.8
          69.0       1.2
          72.0       1.0
          73.0       7.6
          74.0       4.3
          74.5       1.9
          75.0       6.5
          75.5       2.2
          76.0       1.5
          82.0       1.0
          84.0       1.7
          85.0       2.3
          86.0       2.6
          87.0       4.5
          88.0       3.4
          89.0      15.0
          90.0       1.8
          92.5       1.0
          95.5       1.4
          96.0       1.4
          97.0       3.6
          99.0       4.9
         100.0       1.3
         101.0       1.7
         102.0       1.1
         107.0       1.0
         109.0       3.0
         111.0       1.8
         114.0       5.7
         115.0       2.3
         116.0       1.2
         123.0      23.5
         124.0       8.8
         125.0      19.5
         126.0       3.8
         127.0       4.2
         129.0       1.0
         133.0       3.9
         135.0       2.6
         148.0       1.4
         149.0       1.3
         150.0      78.9
         151.0      11.0
         152.0      26.3
         153.0       3.6
         156.0       1.2
         157.0       2.8
         158.0       1.2
         159.0      73.2
         160.0      11.1
         161.0      50.1
         162.0       7.0
         163.0      10.1
         164.0       1.5
         165.0       3.6
         167.0       1.0
         184.0       3.3
         185.0      51.8
         186.0      27.0
         187.0      63.7
         188.0      18.9
         189.0      25.1
         190.0       4.3
         191.0       4.3
         192.0       3.2
         194.0       1.0
         199.0       1.2
         200.0       8.8
         201.0       2.4
         202.0       5.8
         203.0       1.2
         204.0       1.0
         210.0       3.4
         212.0       2.2
         226.0      10.0
         227.0     100.0
         228.0      19.4
         229.0      64.3
         230.0       9.3
         231.0      10.6
         232.0       1.3
    

400 MHz in DMSO-d6 (at 50.C)

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    1H NMR 399.65 MHz
    C9 H7 Cl2 N3 0.041 g : 0.5 ml DMSO-d6 at 50C
    alpha-cyanoimino-3,4-dichlorophenethylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 8.5 B *1 8.4 C 7.60 D 7.60 E 7.33 F 3.71 J(C,E)=8.2HZ

         Hz     ppm     Int.
    

       3338.01   8.353    124
       3056.95   7.650     28
       3056.49   7.648     30
       3055.27   7.645     34
       3052.98   7.640     40
       3052.52   7.638     41
       3052.06   7.637     43
       3042.76   7.614    655
       3034.52   7.593   1000
       3022.61   7.564     34
       3020.78   7.559     27
       2942.20   7.362     33
       2932.74   7.339    295
       2932.28   7.338    295
       2924.80   7.319    259
       2924.35   7.318    259
       1480.71   3.706    189
    

in DMSO-d6 (at 80.C)

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KBr disc

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nujol mull

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