叔戊基胺(594-39-8)核磁图(¹³CNMR)

Mass

MS-NW-5727          
tert-pentylamine
C5H13N              (Mass of molecular ion:     87)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       3.2
      18.0       5.9
      27.0       5.1
      28.0       3.1
      29.0       3.4
      30.0       7.6
      31.0       3.0
      39.0       3.8
      41.0       9.9
      42.0      10.1
      43.0       5.2
      44.0       1.6
      45.0       1.2
      54.0       1.0
      55.0      17.6
      56.0       2.6
      57.0       4.8
      58.0     100.0
      59.0       4.1
      70.0       2.6
      71.0       1.5
      72.0      28.6
      73.0       1.7

Assign. Shift(ppm) A 1.38 B 1.23 C 1.071 D 0.90

     Hz     ppm     Int.

    128.69   1.437     39
    127.94   1.429     35
    122.38   1.367     22
    120.88   1.350     67
    115.00   1.285     30
    113.50   1.268     31
    110.06   1.229    202
    108.75   1.215     56
     97.88   1.093     26
     95.94   1.072   1000
     94.00   1.050     38
     87.69   0.980     53
     86.75   0.969     84
     85.81   0.959     56
     80.00   0.894    220
     79.31   0.886     69
     77.81   0.869     35
     73.19   0.818     30
     72.13   0.806     42
     70.50   0.788     25