1，6-二碘己烷(629-09-4)核磁图(¹³CNMR)

Mass

MS-IW-8666          
1,6-diiodohexane
C6H12I2             (Mass of molecular ion:    338)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0      17.3
      28.0       4.3
      29.0      10.8
      39.0      11.6
      40.0       2.5
      41.0      50.4
      42.0       5.0
      43.0      18.6
      53.0       3.4
      54.0       2.0
      55.0      85.0
      56.0       6.9
      57.0       4.5
      67.0       2.1
      69.0       1.0
      81.0       4.3
      83.0     100.0
      84.0       8.1
     105.5       1.5
     127.0       4.7
     128.0       3.9
     141.0       3.5
     154.0       1.3
     155.0      59.5
     156.0       1.3
     169.0      44.9
     170.0       1.4
     183.0      11.8
     209.0       2.2
     210.0       1.8
     211.0      89.2
     212.0       5.9
     254.0       1.5
     338.0      38.3
     339.0       2.6

Assign. Shift(ppm) A 3.192 B 1.84 C 1.43

     Hz     ppm     Int.

    292.81   3.270    410
    285.94   3.193   1000
    279.13   3.117    607
    179.63   2.006     36
    178.13   1.989     54
    176.94   1.976     57
    175.81   1.964     65
    171.31   1.913    180
    170.75   1.907    178
    165.00   1.843    252
    164.19   1.834    254
    158.25   1.767    218
    152.69   1.705     95
    151.38   1.691    103
    148.75   1.661     54
    148.44   1.658     53
    144.69   1.616     48
    143.56   1.603     43
    141.06   1.576     64
    138.88   1.551     67
    133.88   1.495    249
    130.56   1.458    277
    129.63   1.448    287
    127.00   1.419    365
    124.25   1.388    216
    123.06   1.375    244
    120.69   1.348    127
    119.50   1.335    128