双(4-氯丁基)醚(6334-96-9)核磁图(¹³CNMR)

Mass

MS-NW-3320          
bis(4-chlorobutyl) ether
C8H16Cl2O           (Mass of molecular ion:    198)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      18.0       1.4
      27.0       9.8
      28.0       2.4
      29.0      11.5
      31.0       4.4
      36.0       1.2
      39.0       6.2
      40.0       1.2
      41.0      11.5
      42.0       9.8
      43.0       4.3
      44.0       2.4
      45.0       1.1
      49.0       2.2
      53.0       2.3
      54.0       1.7
      55.0      77.5
      56.0       4.6
      62.0       1.8
      63.0       3.7
      65.0       1.2
      71.0       5.4
      72.0       2.0
      73.0       2.6
      89.0       1.0
      90.0       1.8
      91.0     100.0
      92.0       5.0
      93.0      33.4
      94.0       1.4
     107.0       1.1
     121.0       4.7
     123.0       1.6
     198.0       1.0

Assign. Shift(ppm) A *1 3.56 B *1 3.45 C 2.04 to 1.53

     Hz     ppm     Int.

    327.50   3.657     38
    325.81   3.638    331
    321.81   3.594    153
    320.88   3.583    230
    319.31   3.566   1000
    315.81   3.527    109
    313.81   3.504    555
    313.06   3.496    640
    310.75   3.470    167
    307.88   3.438    901
    305.69   3.414    206
    302.00   3.373    364
    182.50   2.038     32
    179.81   2.008     40
    176.69   1.973     54
    174.56   1.950     86
    173.00   1.932    113
    170.94   1.909    144
    167.94   1.876    218
    166.06   1.855    233
    164.38   1.836    305
    161.75   1.807    406
    160.81   1.796    396
    159.25   1.779    536
    157.94   1.764    437
    156.63   1.749    405
    154.56   1.726    323
    152.94   1.708    255
    152.19   1.700    250
    151.19   1.689    205
    148.38   1.657    166
    146.25   1.633    151
    144.81   1.617     96
    143.25   1.600     57
    142.88   1.596     60
    142.19   1.588     67
    139.81   1.562     42