657-26-1

L-赖氨酸二盐酸盐(657-26-1)核磁图(¹³CNMR)

产品名称:L-赖氨酸二盐酸盐

CAS:657-26-1

分子式:C6H16Cl2N2O2

分子量: 219.11

InChI:InChI=1/C6H14N2O2.2ClH/c7-4-2-1-3-5(8)6(9)10;;/h5H,1-4,7-8H2,(H,9,10);2*1H/t5-;;/s3

InChIKey: JBBURJFZIMRPCZ-WHWWGIJDNA-N

Smiles:[C@@H](N)(C(=O)O)CCCCN.Cl.Cl |&1:0,r|

400 MHz in D2O

90 MHz in D2O

¹H NMR	399.65 MHz
C₆ H₁₄ N₂ O₂	0.037 g : 0.5 ml D₂O
L-lysine dihydrochloride

    Assign.     Shift(ppm)

      B             4.117
      C             3.034
      D     *1      2.03
      E     *1      1.97
      F             1.741
      G             1.54
     
     THE SOLVENT SIGNAL REMOVED.

     Hz     ppm     Int.

   1651.73   4.133    449
   1645.39   4.118    867
   1642.46   4.110    157
   1639.04   4.102    453
   1220.34   3.054    626
   1212.77   3.035   1000
   1204.96   3.016    640
    829.96   2.077    145
    829.71   2.077    145
    824.46   2.063    147
    824.10   2.063    143
    820.92   2.055    231
    818.85   2.049    211
    815.19   2.040    376
    812.74   2.034    189
    810.30   2.028    344
    804.44   2.013    567
    798.22   1.998    499
    793.33   1.986    274
    791.38   1.981    286
    787.60   1.971    344
    783.08   1.960    197
    782.71   1.959    197
    781.13   1.955    258
    773.32   1.935    145
    712.28   1.783    223
    704.47   1.763    710
    696.78   1.744    982
    689.09   1.725    795
    681.52   1.706    320
    636.47   1.593    213
    630.62   1.578    229
    629.03   1.574    282
    625.85   1.566    250
    623.29   1.560    298
    620.97   1.554    338
    618.41   1.548    300
    615.48   1.541    304
    613.04   1.534    372
    610.47   1.528    268
    607.79   1.521    292
    605.10   1.515    310
    602.54   1.508    252
    601.07   1.504    211
    600.10   1.502    233
    597.17   1.495    235
    594.60   1.488    189
    589.36   1.475    161

¹H NMR	89.56 MHz
C₆ H₁₄ N₂ O₂	0.042 g : 0.5 ml D₂O
L-lysine dihydrochloride

    Assign.     Shift(ppm)

      B             4.075
      C             3.024
      D             1.99
      E          1.79 to 1.45
     
     THE SOLVENT SIGNAL REMOVED.

     Hz     ppm     Int.

    371.50   4.149    435
    371.38   4.147    435
    365.50   4.082   1000
    359.25   4.012    581
    278.69   3.112    443
    278.38   3.109    443
    278.00   3.105    423
    271.94   3.037    842
    264.88   2.958    607
    264.50   2.954    623
    182.75   2.041    518
    181.00   2.021    516
    180.25   2.013    494
    177.63   1.984    476
    177.00   1.977    486
    174.63   1.950    844
    172.94   1.931    468
    168.38   1.881    494
    168.19   1.878    494
    157.69   1.761    630
    157.19   1.756    626
    156.38   1.747    593
    156.00   1.742    593
    155.44   1.736    609
    154.94   1.731    609
    154.56   1.726    626
    151.75   1.695    709
    148.00   1.653    889
    147.69   1.650    883
    146.25   1.633    913
    146.06   1.631    913
    144.69   1.616    765
    142.25   1.589    713
    140.56   1.570    617
    140.25   1.566    615

in D2O