709-60-4

3-乙酰苯磺酰氯氟化物(709-60-4)核磁图(¹HNMR)

产品名称:3-乙酰苯磺酰氯氟化物

CAS:709-60-4

分子式:C8H7FO3S

分子量: 202.2027832

Mass

MS-NW-9956          
m-acetylbenzenesulfonyl fluoride
C8H7FO3S            (Mass of molecular ion:    202)

   Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       1.6
      28.0       2.4
      39.0       1.3
      42.0       1.3
      43.0      26.8
      50.0       7.2
      51.0       2.4
      63.0       2.6
      64.0       3.2
      65.0       1.0
      74.0       3.0
      75.0       9.8
      76.0       7.4
      77.0       1.6
      83.0       2.2
      91.0       1.1
      92.0      22.5
      93.0       1.6
      95.0       3.7
     104.0       1.3
     159.0      15.5
     160.0       1.2
     187.0     100.0
     188.0       8.7
     189.0       5.4
     202.0       9.1

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₈ H₇ F O₃ S	0.038 g : 0.5 ml DMSO-d₆
m-acetylbenzenesulfonyl fluoride

    Assign.     Shift(ppm)

      A             8.52
      B             8.51
      C             8.405
      D             7.982
      E             2.719

     Hz     ppm     Int.

   3404.54   8.519    159
   3403.02   8.516    207
   3401.64   8.512     70
   3395.69   8.497     73
   3365.02   8.420     48
   3363.49   8.417     74
   3361.97   8.413     43
   3356.93   8.400     54
   3355.87   8.398     55
   3355.10   8.396     55
   3354.03   8.393     46
   3197.94   8.002     39
   3197.02   8.000     52
   3196.11   7.998     26
   3189.70   7.982     77
   3181.61   7.961     37
   3180.69   7.959     35
   1086.88   2.720   1000
   1083.53   2.712     23

in DMSO-d6