827-54-3

2-乙烯基萘(827-54-3)核磁图(¹³CNMR)

产品名称:2-乙烯基萘

CAS:827-54-3

分子式:C12H10

分子量: 154.21

InChI:InChI=1S/C12H10/c1-2-10-7-8-11-5-3-4-6-12(11)9-10/h2-9H,1H2

InChIKey: KXYAVSFOJVUIHT-UHFFFAOYSA-N

Smiles:C1=C2C(C=CC=C2)=CC=C1C=C

Mass

MS-IW-2287          
2-vinylnaphthalene
C12H10              (Mass of molecular ion:    154)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      39.0       1.0
      50.0       1.5
      51.0       3.1
      63.0       4.0
      64.0       2.8
      74.0       1.6
      75.0       3.0
      75.5       1.1
      76.0      10.3
      76.5       1.7
      77.0       5.4
      89.0       1.0
     101.0       1.6
     102.0       2.3
     115.0       3.5
     126.0       3.5
     127.0       4.8
     128.0       8.5
     129.0       4.8
     139.0       2.3
     141.0       1.1
     142.0       1.0
     150.0       3.0
     151.0       9.5
     152.0      31.8
     153.0      49.8
     154.0     100.0
     155.0      13.2
     156.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₀	0.030 g : 0.5 ml CDCl₃
2-vinylnaphthalene

    Assign.     Shift(ppm)

      A          7.79 to 7.77
      B             7.728
      C             7.622
      D     *1      7.44
      E     *1      7.42
      F             6.867
      G             5.859
      J             5.321

     Hz     ppm     Int.

   3117.19   7.800    387
   3114.87   7.794    672
   3110.96   7.785    977
   3107.91   7.777    729
   3105.35   7.771    472
   3102.17   7.763    737
   3088.75   7.729    785
   3050.90   7.634    527
   3049.19   7.630    508
   3042.36   7.613    390
   3040.65   7.609    381
   2983.40   7.466    117
   2981.81   7.462    162
   2976.56   7.448    466
   2974.73   7.444    456
   2973.14   7.440    563
   2970.09   7.432   1000
   2966.92   7.424    484
   2965.58   7.421    460
   2963.75   7.416    445
   2958.37   7.403    149
   2956.91   7.399    109
   2759.03   6.904    335
   2748.17   6.877    350
   2741.46   6.860    367
   2730.59   6.833    373
   2350.22   5.881    688
   2332.64   5.837    631
   2132.32   5.336    668
   2131.96   5.335    674
   2121.09   5.308    656

in CDCl3