86087-23-2

(S)-(+)-3-羟基四氢呋喃(86087-23-2)核磁图(¹HNMR)

产品名称:(S)-(+)-3-羟基四氢呋喃

CAS:86087-23-2

分子式:C4H8O2

分子量: 88.11

InChI:InChI=1S/C4H8O2/c5-4-1-2-6-3-4/h4-5H,1-3H2/t4-/m0/s1

InChIKey: XDPCNPCKDGQBAN-BYPYZUCNSA-N

Smiles:O1CC[C@H](O)C1

Mass

MS-IW-9526          
(S)-tetrahydro-3-furanol
C4H8O2              (Mass of molecular ion:     88)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      14.0       1.7
      15.0       5.0
      18.0       2.5
      26.0       5.1
      27.0      13.8
      28.0      21.1
      29.0      35.2
      30.0      21.7
      31.0      46.8
      32.0       9.7
      33.0       1.3
      38.0       1.6
      39.0      11.3
      40.0       9.3
      41.0      11.5
      42.0      10.3
      43.0      20.5
      44.0      16.7
      45.0       5.3
      55.0       1.9
      56.0       2.3
      57.0     100.0
      58.0      85.2
      59.0       4.7
      60.0       8.4
      61.0       1.0
      69.0       1.5
      70.0      16.2
      71.0       2.0
      87.0       1.0
      88.0      12.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₄ H₈ O₂	0.05 ml : 0.5 ml CDCl₃
(S)-tetrahydro-3-furanol

    Assign.     Shift(ppm)

      A             4.463
      B             4.00
      C     *1      3.926
      D     *1      3.830
      E     *2      3.775
      F     *2      3.721
      G     *3      2.059
      J     *3      1.908

     Hz     ppm     Int.

   1790.16   4.480    191
   1786.25   4.470    368
   1784.42   4.465    379
   1782.47   4.461    369
   1780.64   4.456    347
   1776.73   4.446    162
   1600.10   4.004    791
   1595.95   3.994    681
   1593.14   3.987    359
   1586.18   3.969    373
   1584.72   3.966    592
   1577.76   3.948    604
   1576.17   3.944    435
   1569.21   3.927    363
   1540.89   3.856    425
   1536.87   3.846    445
   1532.35   3.835    647
   1528.32   3.825    639
   1524.05   3.814    332
   1520.02   3.804    345
   1516.97   3.796    521
   1512.82   3.786    486
   1507.45   3.772   1000
   1503.30   3.762    959
   1491.70   3.733    636
   1490.23   3.729    751
   1488.89   3.726    612
   1482.06   3.709    292
   1480.59   3.705    355
   1479.25   3.702    292
    841.92   2.107    167
    836.18   2.093    180
    833.25   2.085    323
    828.74   2.074    285
    827.51   2.071    353
    824.46   2.063    200
    823.12   2.060    268
    820.07   2.052    467
    818.85   2.049    236
    814.33   2.038    439
    811.40   2.031    232
    805.66   2.016    217
    771.61   1.931    173
    770.63   1.929    200
    769.78   1.927    205
    768.68   1.924    201
    767.70   1.921    208
    766.60   1.919    220
    765.75   1.917    232
    764.77   1.914    315
    763.79   1.912    230
    762.94   1.910    218
    761.84   1.907    205
    760.74   1.904    202
    759.64   1.901    214
    758.79   1.899    272
    757.69   1.896    268
    756.84   1.894    173
    755.62   1.891    150
    754.52   1.888    149
    753.42   1.886    152
    752.56   1.884    157
    751.59   1.881    212
    750.61   1.879    154
    749.76   1.877    143
    748.66   1.874    136
    747.56   1.871    128
    746.46   1.868    129
    745.61   1.866    124
    744.75   1.864    108

in CDCl3