91-88-3

N-乙基-N-羟乙基间甲苯胺(91-88-3)核磁图(¹HNMR)

产品名称:N-乙基-N-羟乙基间甲苯胺

CAS:91-88-3

分子式:C11H17NO

分子量: 179.26

InChI:InChI=1S/C11H17NO/c1-3-12(7-8-13)11-6-4-5-10(2)9-11/h4-6,9,13H,3,7-8H2,1-2H3

InChIKey: KRNUKKZDGDAWBF-UHFFFAOYSA-N

Smiles:C(O)CN(CC)C1=CC=CC(C)=C1

Mass

MS-IW-6283          
2-(N-ethyl-m-toluidino)ethanol
C11H17NO            (Mass of molecular ion:    179)

   Source Temperature: 200 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      29.0       1.0
      39.0       1.3
      65.0       4.1
      77.0       2.3
      89.0       1.1
      91.0      11.1
      92.0       2.6
      93.0       3.0
     105.0       1.9
     118.0       4.9
     119.0       3.1
     120.0      32.0
     121.0       3.1
     133.0       1.2
     134.0       1.4
     147.0       1.1
     148.0     100.0
     149.0      11.3
     164.0       1.9
     179.0      15.9
     180.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₇ N O	0.05 ml : 0.5 ml CDCl₃
2-(n-ethyl-m-toluidino)ethanol

    Assign.     Shift(ppm)

      A             7.089
      B             6.562
      C             6.53
      D             3.700
      E             3.376
      F             3.339
      G             2.42
      J             2.289
      K             1.111

     Hz     ppm     Int.

   2841.31   7.110     84
   2833.50   7.090    168
   2825.93   7.072     98
   2622.56   6.563    391
   2614.99   6.544    135
   2611.45   6.535    190
   2610.84   6.533    187
   2603.15   6.514    145
   1485.35   3.717    226
   1479.25   3.702    468
   1473.27   3.687    267
   1355.71   3.393    249
   1349.49   3.377    478
   1343.51   3.362    249
   1341.80   3.358    374
   1334.72   3.340    344
   1327.76   3.323    125
    966.55   2.419    130
    914.92   2.290   1000
    451.17   1.129    394
    444.09   1.112    752
    437.13   1.094    390

in CDCl3