4,4,5,5,6,6,6-HEPTAFLUORO-1-PHENYL-1,3-HEXANEDIONE synthesis
- Product Name:4,4,5,5,6,6,6-HEPTAFLUORO-1-PHENYL-1,3-HEXANEDIONE
- CAS Number:53580-21-5
- Molecular formula:C12H7F7O2
- Molecular Weight:316.17
356-27-4
103 suppliers
$15.00/5 g
98-86-2
792 suppliers
$9.00/5g
53580-21-5
22 suppliers
$60.00/100mg
Yield: 80%
Reaction Conditions:
Stage #1:ethyl heptafluorobutyrate with sodium methylate in methanol;diethyl ether at 0; for 0.5 h;
Stage #2:acetophenone in methanol;diethyl ether at 20; for 16 h;Further stages.;Claisen condensation;
References:
Büttner, Stefan;Lubbe, Mathias;Reinke, Helmut;Fischer, Christine;Langer, Peter [Tetrahedron,2008,vol. 64,# 34,p. 7968 - 7976]
356-24-1
103 suppliers
$13.00/5g
98-86-2
792 suppliers
$9.00/5g
53580-21-5
22 suppliers
$60.00/100mg