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1-Bromo-2-(2-methoxyethoxy)ethane

1-Bromo-2-(2-methoxyethoxy)ethane structure

CAS No.: 54149-17-6

Chemical Name:: 1-Bromo-2-(2-methoxyethoxy)ethane

Synonyms: DK815;mPEG2-Br;CAS_54149-17-6;Methyl-PEG2-bromide;1-bromo-3,6-dioxaheptane;MONO METHOXY PEG BROMIDE;1-BROMO-(2-METHOXYETHOXY)ETHANE;2-(2-Methoxyethoxy)ethyl bromide;1-BROMO-2-(2-METHOXYETHOXY)ETHANE;1-(2-Bromoethoxy)-2-methoxyethane

CBNumber:: CB2216300

Molecular Formula:: C5H11BrO2

Molecular Weight:: 183.04

MDL Number:: MFCD00000238

MOL File:: 54149-17-6.mol

MSDS File:: SDS

Last updated:2023-11-10 16:48:32

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1-Bromo-2-(2-methoxyethoxy)ethane Properties

Boiling point	156 °C (lit.) 37-40 °C/0.01 mmHg (lit.)
Density	1.3600 g/mL at 25 °C (lit.)
refractive index	n20/D 1.455(lit.)
Flash point	163 °F
storage temp.	2-8°C
form	Liquid
color	Clear colorless to pale yellow
Water Solubility	Not miscible in water.
Sensitive	Light Sensitive
BRN	2069579
InChI	InChI=1S/C5H11BrO2/c1-7-4-5-8-3-2-6/h2-5H2,1H3
InChIKey	HUXJXNSHCKHFIL-UHFFFAOYSA-N
SMILES	C(OCCBr)COC
CAS DataBase Reference	54149-17-6(CAS DataBase Reference)
NIST Chemistry Reference	1-Bromo-2-(2-methoxyethoxy)ethane(54149-17-6)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H227

Precautionary statements

P210e-P280a-P370+P378a-P403+P235-P501a

Risk Statements

36/37/38

Safety Statements

24/25

WGK Germany

HS Code

29091990

NFPA 704

	2
0		0

1-Bromo-2-(2-methoxyethoxy)ethane price More Price(24)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	639842	1-Bromo-2-(2-methoxyethoxy)ethane 95%	54149-17-6	10g	$281	2024-03-01	Buy
Sigma-Aldrich	456195	1-Bromo-2-(2-methoxyethoxy)ethane 90%	54149-17-6	10g	$99	2024-03-01	Buy
TCI Chemical	B4736	1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na2CO3) >90.0%(GC)	54149-17-6	5g	$48	2024-03-01	Buy
TCI Chemical	B4736	1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na2CO3) >90.0%(GC)	54149-17-6	25g	$185	2024-03-01	Buy
Alfa Aesar	L05406	1-Bromo-2-(2-methoxyethoxy)ethane, tech. 90%, stab. with sodium carbonate	54149-17-6	5g	$55.65	2024-03-01	Buy

Product number	Packaging	Price	Buy
639842	10g	$281	Buy
456195	10g	$99	Buy
B4736	5g	$48	Buy
B4736	25g	$185	Buy
L05406	5g	$55.65	Buy

1-Bromo-2-(2-methoxyethoxy)ethane Chemical Properties,Uses,Production

Chemical Properties

clear colorless to pale yellow liquid

Uses

1-Bromo-2-(2-methoxyethoxy)ethane is an important raw material and intermediate used in organic synthesis, pharmaceuticals, agrochemicals and dyestuff.

Synthesis

General Procedure for Preparation of 1-Bromo-2-(2-methoxyethoxy)ethane: Into a 25-mL round bottomed flask equipped with magnetic stir bar, addition funnel and positive flow of nitrogen were placed 15.60 mmol of a ethyleneglycol monomethyl ether. The solution was stirred for 15 min in an ice bath before the dropwise addition of phosphorous tribromide (7.81 mmol) over a 10 min period. The solution was allowed to gradually warm and stir at room temperature (rt) for 14 hrs. The solution was then heated in a 90 °C oil bath for 1 hr, at which time the solution turned yellow. The solution was allowed to cool to rt, poured onto 30 g of ice/water mixture, and made slightly basic with addition of a 10% solution of NaHCO3 (~6 mL). Subsequent extraction with diethyl ether (Et2O) (3 x 30 mL), followed by drying over MgSO4 and concentration under reduced pressure afforded a colorless oil in sufficient purity for use in subsequent reactions.
1-Bromo-2-(2-methoxyethoxy)ethane synthesis

1-Bromo-2-(2-methoxyethoxy)ethane synthesis

Synthesis of 1-Bromo-2-(2-methoxyethoxy)ethane from Diethylene glycol monomethyl ether

1-Bromo-2-(2-methoxyethoxy)ethane Preparation Products And Raw materials

Raw materials

m-PEG3-Tos Diethylene glycol monomethyl ether

Preparation Products

2-(2-Methoxyethoxy)ethanamine Propanedioic acid, 2-[2-(2-methoxyethoxy)ethyl]-, 1,3-diethyl ester {4-[2-(2-Methoxyethoxy)ethoxy]phenyl}methanol 2,5-bis[2-(2-methoxyethoxy)ethoxy]terephthalaldehyde

1-Bromo-2-(2-methoxyethoxy)ethane Suppliers

Global( 154)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	15956	58
Hebei Xinsheng New Material Technology Co., LTD.	+86-16632316109	xinshengkeji@xsmaterial.com	China	1099	58
9i LLC	+18039569191	MWan@NiNeiLab.com	United States	418	58
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21688	55
Zjartschem	+86-571-8723 8903 jocelynpan@zjarts.com	jocelynpan@zjarts.com	CHINA	993	58
Win-Win Chemical CO., Limited	0086-577-64498589	sales@win-winchemical.com	CHINA	998	58
Accela ChemBio Inc.	(+1)-858-699-3322	info@accelachem.com	United States	19965	58
Changzhou Ditong Chemical Co.,Ltd	+86-0519-88299272	info@edengenechem.com	China	2169	58
BAYNOE CHEM CO.,LTD	+86-21-34783353 +8615000719740	baynoe@baynoe.com	CHINA	934	58
CONIER CHEM AND PHARMA LIMITED	+8618523575427	sales@conier.com	China	49391	58

Supplier	Advantage
Shanghai Daken Advanced Materials Co.,Ltd	58
Hebei Xinsheng New Material Technology Co., LTD.	58
9i LLC	58
Henan Tianfu Chemical Co.,Ltd.	55
Zjartschem	58
Win-Win Chemical CO., Limited	58
Accela ChemBio Inc.	58
Changzhou Ditong Chemical Co.,Ltd	58
BAYNOE CHEM CO.,LTD	58
CONIER CHEM AND PHARMA LIMITED	58

View Lastest Price from 1-Bromo-2-(2-methoxyethoxy)ethane manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2023-11-11	1-Bromo-2-(2-methoxyethoxy)ethane 54149-17-6	US $35.00-25.00 / kg	1kg	99%	20 Ton	Hebei Xinsheng New Material Technology Co., LTD.
2023-02-22	1-Bromo-2-(2-methoxyethoxy)ethane 54149-17-6	US $0.00 / KG	1KG	98%min	30tons/month	WUHAN FORTUNA CHEMICAL CO., LTD
2019-12-23	1-Bromo-2-(2-methoxyethoxy)ethane 54149-17-6	US $1.00 / g	1g	99%	1000KGS	Career Henan Chemical Co

1-Bromo-2-(2-methoxyethoxy)ethane
54149-17-6
US $35.00-25.00 / kg
99%
Hebei Xinsheng New Material Technology Co., LTD.

1-Bromo-2-(2-methoxyethoxy)ethane
54149-17-6
US $0.00 / KG
98%min
WUHAN FORTUNA CHEMICAL CO., LTD

1-Bromo-2-(2-methoxyethoxy)ethane
54149-17-6
US $1.00 / g
99%
Career Henan Chemical Co

1-Bromo-2-(2-methoxyethoxy)ethane Spectrum

1-Bromo-2-(2-methoxyethoxy)ethane(54149-17-6)¹HNMR 1-Bromo-2-(2-methoxyethoxy)ethane(54149-17-6)Raman 1-Bromo-2-(2-methoxyethoxy)ethane(54149-17-6)IR 1-Bromo-2-(2-methoxyethoxy)ethane(54149-17-6)FT-IR

54149-17-6(1-Bromo-2-(2-methoxyethoxy)ethane)Related Search:

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2,5,8,11,14,17,20,23,26-Nonaoxaoctacosan-28-amine Methyl-PEG4-t-butyl ester MPEG4-CH2CH2COOH Methyl-PEG6-MS Diethylene glycol monomethyl ether

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1-BROMO-2-(2-METHOXYETHOXY)ETHANE MONO METHOXY PEG BROMIDE Ethane, 1-(2-bromoethoxy)-2-methoxy- 1-BROMO-2-(2-METHOXYETHOXY)ETHANE, TECH. 90%, STAB. WITH SOD 1-BROMO-(2-METHOXYETHOXY)ETHANE 1-Bromo-2-(2-methoxyethoxy)ethane, tech. 90%, stab. with sodium carbonate 1-Bromo-2-(2-methoxyethoxy)ethane, tech. 90% 1-bromo-3,6-dioxaheptane 2-(2-Methoxyethoxy)ethyl bromide 1-BROMO-2-(2-METHOXYETHOXY)ETHANE, 90%, STABILIZED WITH SODIUM CARBONATE 1-Bromo-2-(2-methoxyethoxy)ethane, stabilized with sodium carbonate 1-(2-Bromoethoxy)-2-methoxyethane 2-Bromoethyl 2-methoxyethyl ether 1-Bromo-2-(2-methoxyethoxy)ethane,98% 1-Bromo-2-(2-methoxyethoxy)ethane ,96% 1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na2CO3) 1-Bromo-2-(2-methoxyethoxy)ethane 90% 1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na₂CO₃) 1-Bromo-(2-methoxyethoxy)ethane (stabilised with sodium carbonate) Ethylene Glycol 2-Bromoethyl Methyl Ether Ethane,1-bromo-2-(2-methoxyethoxy)- 1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na2CO3) > 1-Bromo-2-(2-Methoxyethoxy)Ethane, Stab. With Sodium Carbonate mPEG2-Br CAS_54149-17-6 Methyl-PEG2-bromide DK815 1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na?CO?) 54149-17-6 C5H11BrO2 CH3OCH2CH22Br HALOGEN Oxygen Compounds Organic Building Blocks Ethers Building Blocks Ethers Organic Building Blocks Oxygen Compounds