Hesperidin dihydrochalcone

Hesperidin dihydrochalcone 구조식 이미지
카스 번호:
35573-79-6
상품명:
Hesperidin dihydrochalcone
동의어(영문):
Hesperidin Impurity 1 (Hesperidin Dihydrochalcone);1-Propanone, 1-[4-[[6-O-(6-deoxy-α-L-mannopyranosyl)-β-D-glucopyranosyl]oxy]-2,6-dihydroxyphenyl]-3-(3-hydroxy-4-methoxyphenyl)-
CBNumber:
CB53053945
분자식:
C28H36O15
포뮬러 무게:
612.58
MOL 파일:
35573-79-6.mol

Hesperidin dihydrochalcone 속성

끓는 점
923.7±65.0 °C(Predicted)
밀도
1.61±0.1 g/cm3(Predicted)
산도 계수 (pKa)
6.85±0.40(Predicted)

안전

Hesperidin dihydrochalcone C화학적 특성, 용도, 생산

용도

Hesperidin dihydrochalcone can be used as organic intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis

In a stainless steel autoclave, 100 g of hesperidin, 500 ml of 30% liquid sodium hydroxide, and 10 g of pt / c5% wet product were added. Seal well, replace three times with N2 and three times with hydrogen. The pressure is controlled at 1.5Mpa, the temperature is controlled at about 30-90 ° C, and the reaction takes about 10 hours to generate hesperidin dihydrochalcone, which is filtered and the catalyst is continuously reused. According to liquid chromatography analysis, hesperidin dihydrochalcone The yield of ketone was 93%.The reaction solution was neutralized with 31% HCl to neutrality, and then filtered. The filter cake was added to 300 ml of water and heated to complete dissolution, and then cooled to about 10 ° C, and filtered to obtain a white powdered hesperidin dihydrochalcone. The finished product was dried and had a dry weight of 90 g.

Hesperidin dihydrochalcone 준비 용품 및 원자재

원자재

준비 용품


Hesperidin dihydrochalcone 공급 업체

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