477-29-2 Basic information More..
Product Name:COLCHICOSIDE
Synonyms:Colchicine EP impurity D (Colchicoside);(S)-7-Acetylamino-6,7-dihydro-3-(β-D-glucopyranosyloxy)-1,2,10-trimethoxybenzo[a]heptalen-9(5H)-one;Aids012001;Aids-012001;N-[3-(Hexopyranosyloxy)-1,2,10-trimethoxy-9-oxo-5,6,7,9-tetrahydrobenzo[A]heptalen-7-yl]acetamide;Nsc32992;Nsc624672;(S)-N-[3-(β-D-Glucopyranosyloxy)-5,6,7,9-tetrahydro-1,2,10-triMethoxy-9-oxobenzo[a]heptalen-7-yl]acetaMide
CAS:477-29-2
MF:C27H33NO11
MW:547.554
EINECS:207-513-0
Mol File:477-29-2.mol
477-29-2

Use

Purify colchicoside by chromatography through alumina and eluting with CHCl3, then recrystallising from Me2CO, m 275-280o (after releasing solvent at 180o). It also crystallises from EtOH; see colchicine. The tetraacetate has m 175-177o, [] D 15 -57o (c 1, CHCl3). [Bellet et al. Ann Pharm Fr 10 241 1952, Chem Abstr 47 3323 1953, Beilstein 14 IV 946 for colchicine.]

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