- M-PEG3-SH
-
- $0.00 / 5g
-
2024-03-27
- CAS:31521-83-2
- Min. Order: 5g
- Purity: >98.00%
- Supply Ability: 5g
|
| 2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol Basic information |
Product Name: | 2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol | Synonyms: | 2-Methoxy[2-ethoxy(2-ethoxy)]-1-ethanethiol;m-PEG3-thiol;Thiol-PEG3-methyl;MPEG3-SH;2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol;2-<2-(2-methoxyethoxy)ethoxy>ethylthiol;Ethanethiol, 2-[2-(2-methoxyethoxy)ethoxy]-;1-(1-Ethoxyethoxy)-2-methoxyethanethiol | CAS: | 31521-83-2 | MF: | C7H16O3S | MW: | 180.27 | EINECS: | | Product Categories: | peg | Mol File: | 31521-83-2.mol | |
| 2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol Chemical Properties |
Boiling point | 50 °C(Press: 1 Torr) | density | 1.017 | pka | 9.65±0.10(Predicted) |
| 2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol Usage And Synthesis |
Uses | 2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol can be used to prepare biofunctional silicon nanoparticles for drug delivery. | Synthesis | Toluene-4-sulfonic acid 2-[2-(2-methoxyethoxy)-ethoxy]-ethyl ester (2.7) (10.8 g, 34 mmol) and
thiourea (2.6 g, 34 mmol) were dissolved in a mixture of absolute EtOH (20 mL) and H2O (14
mL) and the mixture was refluxed for 3h. 4N NaOH solution (10 mL) was added to mixture and
the reaction mixture refluxed 2 more h. The reaction mixture was concentrated under reduced
pressure to ~ 10 mL, diluted with distilled H2O (10 mL) and neutralized with concentrated HCl.
The solution was extracted with CH2Cl2 (3x10mL) and the solvent was evaporated under
reduced pressure. The pink-yellow liquid was distilled at 0.45 torr pressure. The product was
collected as a clear liquid and obtained in 54% yield. B.p. 55-57 °C at 0.45 torr. GC-MS Calcd.
C7H16O3S+
: 180.0; found: 179.9. 1
H NMR (250 MHz, CDCl3) δ 3.6(6H), 3.5(4H), 3.4(3H),
2.7(2H), 1.6(1H); 13
C NMR (300 MHz, CDCl3) δ 76.92, 73.30, 72.34, 70.98, 70.63, 59.46, 24.66 |
| 2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol Preparation Products And Raw materials |
|
Tag:2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol(31521-83-2)
Related Product Information
|
m-PEG3-Tos
FMOC-21-AMINO-4,7,10,13,16,19-HEXAOXAHENEICOSANOIC ACID
N3-PEG4-tBu
ALPHA,OMEGA-BIS(2-CARBOXYETHYL)POLYETHYLENE GLYCOL 10'000
HO-PEG5-tBu
9-biotinlaMino-4,7-dioxanonanoic acid N-hydroxysucciniMidyl ester
FMOC-12-AMINO-4,7,10-TRIOXADODECANOIC ACID
Maleimide-PEG2-NHS Ester
2,5,8,11,14,17,20,23,26,29,32,35,38,41,44,47-Hexadecaoxanonatetracontan-49-ol
15-[D(+)-BIOTINYLAMINO]-4,7,10,13-TETRAOXAPENTADECANOIC ACID
BOC-15-AMINO-4,7,10,13-TETRAOXAPENTADECANOIC ACID
TERT-BUTYL 12-AMINO-4 7 10-TRIOXA-DODECA
(+)-Biotin-PEG12-CH2CH2COONHS Ester
22-Amino-5,8,11,14,17,20-hexaoxa-2-azadocosanoic acid 1,1-dimethylethyl ester
α,ω-dipropionic acid tetraethylene glycol
O-(2-AMinoethyl)-O'-[2-(Boc-aMino)ethyl]tetraethylene Glycol
H2N-PEG2-tBu
Biotin-PEG4-N3
|