1-Bromooctadecane NEW

English name: 1-Bromooctadecane

CAS number: 112-89-0

Molecular formula: C18H37Br

Molecular weight: 333.39

EINECS number: 204-013-4

MDL No. : MFCD00000231

Stats

Melting point 25-30 °C(lit.)

Boiling point 214-216 °C12 mm Hg(lit.)

Density 0.976 g/mL at 25 °C(lit.)

Refractive index 1.462-1.464

Flash point >230 °F

Storage conditions Inert atmosphere,Room Temperature

The form is Low Melting Solid

Specific gravity 0.980 (20/4℃)

Color Yellow

Water is insoluble

BRN774145

InChIKeyWSULSMOGMLRGKU-UHFFFAOYSA-N

Safety information

GHS hazard pictograms GHS Hazard pictograms

GHS08

Danger

Hazard Description H304

Precautions P301+P310-P331-P405-P501

Hazard category code 36/37/38

Safety Instructions 22-24/25

WGK Germany3

TSCAYes

Customs Code 29033036

Production method:

It is obtained by the reaction of octadecyl alcohol with hydrogen bromide. The alcohol is heated to 100 ° C, the dry hydrogen bromide is added, and the reaction temperature is maintained at 100-120 ° C until the solution no longer absorbs the hydrogen bromide. The bromide was stratified, washed with organic and concentrated sulfuric acid. The bromide removed from the acid was mixed with 90% methanol of the same volume, washed with ammonia to make the bromide alkaline, washed with 90% methanol and dried with anhydrous calcium chloride. Finally, vacuum distillation, collection of 209-211℃ (1.33kPa) fraction is the finished product, the yield of 90%.