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Back ChemicalBook Home>CAS DataBase List>4214-74-8More Spectrum> 2-Amino-3,5-dichloropyridine(4214-74-8) 1H NMR

4214-74-8

2-Amino-3,5-dichloropyridine(4214-74-8) 1H NMR

Molecular FormulaC5H4Cl2N2

Molecular Weight163

InChIInChI=1S/C5H4Cl2N2/c6-3-1-4(7)5(8)9-2-3/h1-2H,(H2,8,9)

InChIKey OCWBGKZFOYMCCN-UHFFFAOYSA-N

SmilesC1(N)=NC=C(Cl)C=C1Cl

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR
    Mass

    MS2016-05371CM      
    3,5-dichloro-2-pyridylamine
    C5H4Cl2N2           (Mass of molecular ion:    162)
    

       Source Temperature: 245 °C
       Sample Temperature:  20 °C
       Direct, 70 eV
    

          18.0       1.7
          28.0       5.1
          37.0       3.5
          38.0       2.6
          49.0       1.9
          50.0       3.7
          52.0       2.3
          62.0       1.4
          63.5       2.7
          64.0       5.4
          65.0       4.8
          72.0       4.5
          73.0       7.6
          74.0       2.9
          75.0       4.9
          84.0       1.5
          85.0       1.8
          91.0       2.7
          92.0       9.4
          98.0       2.0
          99.0       3.5
         100.0      13.8
         101.0       1.9
         102.0       5.4
         107.0       3.9
         108.0       4.0
         109.0       2.8
         110.0       2.8
         126.0       2.7
         127.0      37.9
         128.0       3.4
         129.0      12.3
         134.0       3.6
         135.0      29.8
         136.0       3.7
         137.0      19.1
         139.0       3.0
         162.0     100.0
         163.0       6.8
         164.0      63.0
         165.0       4.1
         166.0      10.1
    

90 MHz in CDCl3

parameter in CDCl3

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR

    1H NMR 89.56 MHz
    C5 H4 Cl2 N2 0.040 g : 0.5 ml CDCl3
    3,5-dichloro-2-pyridylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.938 B 7.501 C 4.9 J(A,B)=2.2HZ

         Hz     ppm     Int.
    

        712.13   7.952    488
        709.94   7.927    555
        672.94   7.514   1000
        670.69   7.489    902
        439.75   4.911     97
    

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR

    1H NMR 300 MHz
    C5 H4 Cl2 N2 0.040 g : 0.5 ml CDCl3
    3,5-dichloro-2-pyridylamine
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 7.938 D(B) 7.501 J(A,B) 2.22 D(C) 4.90

         Hz     ppm     Int.
    

       2382.52   7.942    698
       2380.33   7.934    719
       2251.40   7.505   1000
       2249.22   7.497    969
       1469.99   4.900    195
    

in CDCl3

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR

KBr disc

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR

liquid film

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR

nujol mull

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR

  • 2-Amino-3,5-dichloropyridine(4214-74-8) <sup>1</sup>H NMR

2-Amino-3,5-dichloropyridine(4214-74-8) 1H NMR Atlas of Related Products

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