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[1,1'-Biphenyl]-2-carboxylic acid, 4'-(1,1-dimethylethyl)-, methyl ester synthesis

4synthesis methods
610-97-9 Synthesis
Methyl 2-iodobenzoate

610-97-9
415 suppliers
$9.00/1g

123324-71-0 Synthesis
4-tert-Butylphenylboronic acid

123324-71-0
394 suppliers
$5.00/1g

[1,1'-Biphenyl]-2-carboxylic acid, 4'-(1,1-dimethylethyl)-, methyl ester

1528793-37-4
2 suppliers
inquiry

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Yield:1528793-37-4 100%

Reaction Conditions:

with bis(triphenylphosphine)palladium(II) dichloride;sodium carbonate in tetrahydrofuran;water at 80; for 14 h;Schlenk technique;Inert atmosphere;Sealed tube;Suzuki-Miyaura Coupling;

References:

Morack, Tobias;Metternich, Jan B.;Gilmour, Ryan [Organic Letters,2018,vol. 20,# 5,p. 1316 - 1319] Location in patent:supporting information

123324-71-0 Synthesis
4-tert-Butylphenylboronic acid

123324-71-0
394 suppliers
$5.00/1g

[1,1'-Biphenyl]-2-carboxylic acid, 4'-(1,1-dimethylethyl)-, methyl ester

1528793-37-4
2 suppliers
inquiry

3972-65-4 Synthesis
1-Bromo-4-tert-butylbenzene

3972-65-4
319 suppliers
$8.00/10g

653589-95-8 Synthesis
METHYL 2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZOATE

653589-95-8
123 suppliers
$19.00/1g

[1,1'-Biphenyl]-2-carboxylic acid, 4'-(1,1-dimethylethyl)-, methyl ester

1528793-37-4
2 suppliers
inquiry