1H-Benzimidazole-5-carboxylicacid,6-amino-,methylester synthesis

3synthesis methods

Product Name:1H-Benzimidazole-5-carboxylicacid,6-amino-,methylester
CAS Number:181284-95-7
Molecular formula:C9H9N3O2
Molecular Weight:191.1867

15788-16-6
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1H-Benzimidazole-5-carboxylicacid,6-amino-,methylester

181284-95-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 96 percent / SOCl₂ / 12 h / 50 °C
2: 68 percent / HNO₃ / H₂SO₄ / 12 h / 50 °C
3: 98 percent / H₂ / Pd/C / acetic acid / 1 h / Heating

References:

Meyer, Emmanuel A.;Donati, Nicola;Guillot, Marine;Schweizer, W. Bernd;Diederich, Francois;Stengl, Bernhard;Brenk, Ruth;Reuter, Klaus;Klebe, Gerhard [Helvetica Chimica Acta,2006,vol. 89,# 4,p. 573 - 581]

Methyl 6-nitro-1H-benzo[d]iMidazole-5-carboxylate

895581-42-7
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181284-95-7
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References

26663-77-4 Synthesis

26663-77-4
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181284-95-7
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References

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