4-Pyridineboronic acid pinacol ester synthesis
- Product Name:4-Pyridineboronic acid pinacol ester
- CAS Number:181219-01-2
- Molecular formula:C11H16BNO2
- Molecular Weight:205.06
76-09-5
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1692-15-5
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181219-01-2
243 suppliers
$13.00/1g
Yield:-
Reaction Conditions:
with magnesium sulfate in 1,4-dioxane at 110; for 24 h;
Steps:
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine was synthesized by stirring the mixture of pyridin-4-ylboronic acid (11.76 g, 96 mmol), pinacol (13.57 g, 115 mmol), 1,4-dioxane (300 ml) and MgSO4 (15 g) at 110 oC for 1 day. The precipitate was removed by filtration, and after the removal of solvent under reduced pressure, 6 was obtained.
References:
Song, Tao;Rao, Xingtang;Cui, Yuanjing;Yang, Yu;Qian, Guodong [Journal of Alloys and Compounds,2013,vol. 555,p. 22 - 27]
76-09-5
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15854-87-2
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688-74-4
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181219-01-2
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110-86-1
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73183-34-3
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181219-01-2
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110-86-1
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73183-34-3
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1012085-50-5
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181219-01-2
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$13.00/1g
110-86-1
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73183-34-3
556 suppliers
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181219-01-2
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$13.00/1g
329214-79-1
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