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ChemicalBook CAS DataBase List 1,5-Dimethylhexylamine

1,5-Dimethylhexylamine synthesis

5synthesis methods
1,5-Dimethylhexylamine was synthesized from 6-methyl-2-heptanone ([928-68-7]) by amination and catalytic hydrogenation.
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Yield:1569-60-4 73 %Chromat. ,22462-79-9 15 %Chromat. ,543-82-8 5 %Chromat.

Reaction Conditions:

with ammonia;hydrogen in tert-butyl alcohol at 120; for 24 h;Autoclave;High pressure;

References:

Murugesan, Kathiravan;Beller, Matthias;Jagadeesh, Rajenahally V. [Angewandte Chemie - International Edition,2019,vol. 58,# 15,p. 5064 - 5068][Angew. Chem.,2019,vol. 131,# 15,p. 5118 - 5122,5] Location in patent:supporting information

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