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ChemicalBook CAS DataBase List Chlorobutanol

Chlorobutanol synthesis

5synthesis methods
Chlorobutanol is prepared by condensing acetone and chloroform in the presence of solid potassium hydroxide.
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Yield:57-15-8 82%

Reaction Conditions:

with potassium tert-butylate;ammonia at -75 - -65; for 0.5 h;

References:

Bal'on, Ya. G.;Shul'man, M. D.;Vakulenko, L. I. [Journal of Organic Chemistry USSR (English Translation),1989,vol. 25,# 7.1,p. 1231 - 1237][Zhurnal Organicheskoi Khimii,1989,vol. 25,# 7,p. 1369 - 1376]

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