DIALLYLAMINE HYDROCHLORIDE synthesis

Yield:-

Reaction Conditions:

with hydrogenchloride in water at 20;

Steps:

1.2 2. Preparation of diallylamine hydrochloride
Pump the diallylamine into the kettle and start stirring.Pass the jacket cooling water to lower the temperature of the kettle to below 20 °C, pump the hydrochloric acid into the high tank, and slowly add hydrochloric acid at normal pressure.The molar ratio of N-methyldiallylamine to hydrochloric acid is 1:1, and the mixture is kept for 1-2 hours after the dropwise addition, and the reaction is completed to obtain diallylamine hydrochloride.

References:

Zouping Mingxing Chemical Co., Ltd.;Chen Qiang;Zhang Peng;Xu Xiaobo;Wang Tao;Sun Fantong;Du Xiaoyang;Zhang Junling CN109369413, 2019, A Location in patent:Paragraph 0047; 0054; 0055