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ChemicalBook CAS DataBase List M-TyraMine HydrobroMide

M-TyraMine HydrobroMide synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: ethanol; water / 3 h / Inert atmosphere; Reflux
2: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere
3: hydrogen bromide / water / 1.5 h / Inert atmosphere; Reflux

References:

Pignataro, Luca;Boghi, Michele;Civera, Monica;Carboni, Stefano;Piarulli, Umberto;Gennari, Cesare [Chemistry - A European Journal,2012,vol. 18,# 5,p. 1383 - 1400]