![](/CAS/GIF/596-31-6.gif)
METHYL TRIPHENYLMETHYL ETHER synthesis
- Product Name:METHYL TRIPHENYLMETHYL ETHER
- CAS Number:596-31-6
- Molecular formula:C20H18O
- Molecular Weight:274.36
![Triphenylmethanol](/CAS/GIF/76-84-6.gif)
76-84-6
416 suppliers
$6.00/25g
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74-88-4
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$15.00/10g
![METHYL TRIPHENYLMETHYL ETHER](/CAS/GIF/596-31-6.gif)
596-31-6
79 suppliers
$110.00/100mg
Yield: 71%
Reaction Conditions:
with sodium hydride in tetrahydrofuran;mineral oil at 20; for 15 h;
Steps:
3.1.9. 2-Phenyl-2-methoxypropane (6a)
General procedure: To a solution of 2-phenyl-2-propanol (1c) (1.413 g,10.4 mmol) inTHF (20 mL) was added NaH (60 wt% oil dispersion) (1.422 g,35.6 mmol) and MeI (4.755 g, 33.5 mmol) at room temperature, andthe mixture was stirred for 15 h at that temperature. To the reactionmixture was added H2O (30 mL). After being extracted with EtOAc(30 mL 3), the organic layer was dried with MgSO4. After theconcentration, the residue was subject to column chromatographyon SiO2 (hexane: EtOAc 9: 1) to give 2-phenyl-2-methoxypropane (0.850 g, 5.66 mmol, 54%) as colorless oil.
References:
Matsumoto, Shoji;Naito, Masafumi;Oseki, Takehisa;Akazome, Motohiro;Otani, Yasuhiko [Tetrahedron,2017,vol. 73,# 52,p. 7254 - 7259]
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inquiry
![METHYL TRIPHENYLMETHYL ETHER](/CAS/GIF/596-31-6.gif)
596-31-6
79 suppliers
$110.00/100mg
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$110.00/100mg
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![METHYL TRIPHENYLMETHYL ETHER](/CAS/GIF/596-31-6.gif)
596-31-6
79 suppliers
$110.00/100mg