ChemicalBook CAS DataBase List PHENYL METHACRYLATE

PHENYL METHACRYLATE synthesis

12synthesis methods

Product Name:PHENYL METHACRYLATE
CAS Number:2177-70-0
Molecular formula:C10H10O2
Molecular Weight:162.19

760-93-0 Synthesis

760-93-0
302 suppliers
$28.46/50g

108-95-2 Synthesis

108-95-2
719 suppliers
$14.00/25g

2177-70-0
122 suppliers
$8.00/5g

Yield:2177-70-0 99.1%

Reaction Conditions:

with sulfuric acid at 80; for 8 h;Product distribution / selectivity;

Steps:

19.B

(Step (B)) 696 g (7.4 mol) of phenol and 35 g (0.35 mol) of 98 mass % sulfuric acid were added to the 3 L flask containing the above reaction liquid, and the mixture was heated to 80°C, with air bubbled, and then reacted for 8 hours. The methacrylic anhydride disappeared completely. The yield of phenyl methacrylate based on the methacrylic anhydride (calculated by dividing the number of moles of the phenyl methacrylate at the completion of the reaction by the number of moles of the methacrylic anhydride and multiplying the result by 100) at this time was 99.1 %, and the contained methacrylic acid was 823 g.

References:

EP2308820,2011,A1 Location in patent:Page/Page column 22