Pivaldehyde synthesis
- Product Name:Pivaldehyde
- CAS Number:630-19-3
- Molecular formula:C5H10O
- Molecular Weight:86.13
Yield:630-19-3 93%
Reaction Conditions:
in dichloromethane;
Steps:
5 Pivalaldehyde
EXAMPLE 5 Pivalaldehyde Neopentyl alcohol was reacted as in example 2. Solution 1 consisted of 363 g of neopentyl alcohol and 48 g of 4-acetamido-TEMPO in 1 l of methylene chloride. The pumping rate was 30 l/h for solution 1, 22 l/h for solution 2 and 0.5 l/h for solution 3. Yield: 93% (1H-NMR standard analysis).
References:
US2003/73871,2003,A1
3282-30-2
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