6-Chloro-1-tetralone
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6-Chloro-1-tetralone 속성
- 녹는점
- 53 °C
- 끓는 점
- 150°C/0.7mmHg(lit.)
- 밀도
- 1.248±0.06 g/cm3(Predicted)
- 굴절률
- 1.59
- 저장 조건
- Keep in dark place,Sealed in dry,Room Temperature
- 물리적 상태
- powder to lump
- 색상
- 흰색에서 노란색, 주황색으로
- CAS 데이터베이스
- 26673-31-4
6-Chloro-1-tetralone C화학적 특성, 용도, 생산
용도
6-Chloro-1-tetralone is a novel and potent intermediate used for synthesis of pharmaceutical compounds.Synthesis
A solution of sodium nitrite (173 mg, 2.51 mmol) in water (5 mL) at 0 °C (ice-bath) was added to a magnetically stirred suspension of 6-Amino-1-tetralone (360 mg, 2.23 mmol) in aqueous hydrochloric acid (10 mL, 6 M) at 0 °C. This reaction mixture was added dropwise to a solution of copper(I) chloride (267 mg, 2.70 mmol) in concentrated hydrochloric acid (5 mL) at 0 °C. It was allowed to warm up to room 100 temperature and stirred for a further 2 h after which it was neutralised with solid sodium carbonate, extracted with ethyl acetate (3 × 20 mL) and concentrated in vacuo to give slightly yellow oil. This material was subjected to flash chromatography (50% chloroform in hexane) and concentration of the appropriate fractions afforded 6-chloro-1-tetralone (180 mg, 45%) as a waxy solid.6-Chloro-1-tetralone 준비 용품 및 원자재
원자재
준비 용품
6-Chloro-1-tetralone 공급 업체
글로벌( 204)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Affinity(Wuhan)Ltd. | +86-+undefined-0411-39805809 +86-+undefined-15841022315 |
sales@affinitytech.cn | China | 126 | 58 |
Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 |
info@fdachem.com | China | 16805 | 58 |
Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 |
sales@capotchem.com | China | 29797 | 60 |
Hangzhou FandaChem Co.,Ltd. | 008657128800458; +8615858145714 |
fandachem@gmail.com | China | 9346 | 55 |
career henan chemical co | +86-0371-86658258 |
sales@coreychem.com | China | 29914 | 58 |
Accela ChemBio Inc. | (+1)-858-699-3322 |
info@accelachem.com | United States | 19965 | 58 |
Changzhou Ditong Chemical Co.,Ltd | +86-0519-88299272 |
info@edengenechem.com | China | 2169 | 58 |
BTC Nantong Pharmaceuticals Technology Co.,Ltd | +8618068193575 |
sales4@btcpharm.com | China | 254 | 58 |
Chongqing Chemdad Co., Ltd | +86-023-61398051 +8613650506873 |
sales@chemdad.com | China | 39916 | 58 |
CONIER CHEM AND PHARMA LIMITED | +8618523575427 |
sales@conier.com | China | 49390 | 58 |
6-Chloro-1-tetralone 관련 검색:
데카하이드로나프탈렌 1-클로로나프탈렌 에피클로로하이드린 테트라히드로나프탈렌 트라조돈 디하이드로미르세놀 클로로디플루오르메탄 클로로아세트산
1-Tetralone
Nabumetone
Chlortalidone
Chlormezanone
beta-Tetralone
5-Chloro-2-tetralone,7-Chloro-2-tetralone
6-CHLORO-2-TETRALONE
6,7-Dichloro-2-tetralone
8-Chloro-1-tetralone,8-Chloro-α-Tetralone,8-CHLORO-A-TETRALONE
KETAMINE/ZYLAZINE SOLUTION--SCHEDULE*III ITEM