5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠

5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠
5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠 구조식 이미지
카스 번호:
511540-64-0
한글명:
5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠
동의어(한글):
5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠
상품명:
5-((4-BroMo-2,6-difluorophenyl)difluoroMethoxy)-1,2,3-trifluorobenzene
동의어(영문):
(4-bromo-2,6-difluorophenyl)(difluoro)methyl 3,4,5-trifluoro...;5-Bromo-2-(difluoro(3,4,5-trifluorophenoxy)methyl)-1,3-difluorobenzen;5-bromo-2-(difluoro(3,4,5-trifluorophenoxy)methyl)-1,3-difluorobenzene;5-((4-BroMo-2,6-difluorophenyl)difluoroMethoxy)-1,2,3-trifluorobenzene;(4-bromo-2,6-difluorophenyl)(difluoro)methyl 3,4,5-trifluorophenyl ether;5-Bromo-2-(Di‐ Fluoro(3,4,5-Trifluoromethoxy)methyl)-1,3-Difluorobenzene;Benzene, 5-[(4-bromo-2,6-difluorophenyl)difluoromethoxy]-1,2,3-trifluoro-
CBNumber:
CB42561402
분자식:
C13H4BrF7O
포뮬러 무게:
389.06
MOL 파일:
511540-64-0.mol

5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠 속성

끓는 점
334.6±37.0 °C(Predicted)
밀도
1.743±0.06 g/cm3(Predicted)
증기압
0.019-5.4Pa at 20-50℃
물리적 상태
고체
물리적 상태
단단한 모양
색상
하얀색
LogP
5.7 at 25℃ and pH7

안전

5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠 C화학적 특성, 용도, 생산

화학적 성질

white powder

제조 방법

The preparation of 5-((4-BroMo-2,6-difluorophenyl)difluoroMethoxy)-1,2,3-trifluorobenzene is as follows:Under nitrogen, the three-fluorophenyl 0-3,4,5-2,6-difluoro-4- bromophenyl thioformate 1L 4-neck flask was added 109.0g, 220mLdichloroethane was added to dissolve burning, system is heated to 60 ° C, 30%tetrahydrofuran solution of hydrofluoric acid added to the system 190.0g,250.8g of bromine was slowly dropped to the system, after dropping heatstirring 4h. Thereto was added a saturated sodium bicarbonate solution wasquenched standing layer, the aqueous phase was extracted twice with l00mLdichloroethane, the combined organic phase was washed with water and dried offthe solvent, the crude product 125 · 3g. The crudeproduct is recrystallized from ethanol 250mL white solid 105.1g, detected by GC98.9%, to close It was 95.0%.

511540-64-0.png

5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠 준비 용품 및 원자재

원자재

준비 용품


5-((4-브로모-2,6-디플루오로페닐)디플루오로메톡시)-1,2,3-트리플루오로벤젠 공급 업체

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