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返回ChemicalBook首页>CAS数据库列表>10061-68-4更多图谱> N,N'-二乙基-1,3-丙二胺(10061-68-4)核磁图(13CNMR)

10061-68-4

N,N'-二乙基-1,3-丙二胺(10061-68-4)核磁图(13CNMR)

分子式:C7H18N2

分子量: 130.23

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    Mass

    MS-NW-9731          
    N,N'-diethyltrimethylenediamine
    C7H18N2             (Mass of molecular ion:    130)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.0
          18.0       3.2
          27.0       4.7
          28.0      13.2
          29.0       8.8
          30.0      58.0
          31.0       1.0
          39.0       1.4
          41.0       6.7
          42.0       8.6
          43.0       4.6
          44.0      25.8
          45.0      12.9
          46.0       1.3
          50.0       6.3
          54.0       1.1
          56.0      18.5
          57.0       7.0
          58.0     100.0
          59.0       4.9
          68.0       1.2
          70.0      91.2
          71.0       6.7
          72.0      19.3
          73.0       1.5
          84.0       8.7
          85.0      72.6
          86.0       6.3
          87.0       6.7
         130.0       1.2
         131.0       2.2
         141.0       3.1
    

400 MHz in CDCl3

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    1H NMR 399.65 MHz
    C7 H18 N2 0.05 ml : 0.5 ml CDCl3
    N,N'-diethyltrimethylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.676 B 2.645 C 1.691 D 1.46 E 1.105

         Hz     ppm     Int.
    

       1076.90   2.695    355
       1069.82   2.677    594
       1067.87   2.673    289
       1062.87   2.660    404
       1060.67   2.654    642
       1057.01   2.645     40
       1053.47   2.636    639
       1050.17   2.628     36
       1046.39   2.619    262
        689.82   1.727     56
        682.74   1.709    188
        675.66   1.691    244
        668.58   1.673    171
        661.74   1.656     53
        583.01   1.459    145
        448.97   1.124    610
        441.77   1.106   1000
        434.69   1.088    669
    

in CDCl3

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liquid film

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