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返回ChemicalBook首页>CAS数据库列表>28712-62-1更多图谱> 3-甲基-5,6,7,8-四氢喹啉(28712-62-1)核磁图(1HNMR)

28712-62-1

3-甲基-5,6,7,8-四氢喹啉(28712-62-1)核磁图(1HNMR)

分子式:C10H13N

分子量: 147.22

InChI:InChI=1S/C10H13N/c1-8-6-9-4-2-3-5-10(9)11-7-8/h6-7H,2-5H2,1H3

InChIKey: GMMKZUPOLVXWFF-UHFFFAOYSA-N

Smiles:N1C2=C(CCCC2)C=C(C)C=1

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    Mass

    MS-IW-1361          
    3-methyl-5,6,7,8-tetrahydroquinoline
    C10H13N             (Mass of molecular ion:    147)
    

       Source Temperature: 230 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          27.0       1.4
          39.0       4.8
          41.0       1.7
          50.0       1.5
          51.0       4.3
          52.0       2.3
          53.0       2.4
          63.0       2.6
          65.0       4.9
          65.5       1.3
          66.0       1.8
          71.5       1.3
          72.5       1.1
          77.0       8.1
          78.0       3.4
          79.0       3.3
          89.0       1.6
          90.0       1.0
          91.0       7.4
          92.0       2.4
          93.0       4.5
         103.0       2.2
         104.0       7.4
         105.0       2.1
         106.0       4.5
         107.0       1.5
         115.0       3.2
         116.0       1.5
         117.0       8.0
         118.0      10.2
         119.0      31.7
         120.0       4.6
         121.0       1.1
         128.0       1.2
         129.0       1.4
         130.0       7.8
         131.0      16.0
         132.0      34.2
         133.0       3.8
         143.0       2.3
         144.0      10.4
         145.0       3.4
         146.0     100.0
         147.0      96.6
         148.0      11.5
    

400 MHz in CDCl3

90 MHz in CDCl3

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    1H NMR 399.65 MHz
    C10 H13 N 20.8 mg : 0.5 ml CDCl3
    3-methyl-5,6,7,8-tetrahydroquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.176 B 7.157 C 2.875 D 2.721 E 2.252 F 1.873 G 1.787

         Hz     ppm     Int.
    

       3268.07   8.178    166
       3267.33   8.176    163
       3266.72   8.174    168
       2860.96   7.159    173
       2860.47   7.158    171
       2859.99   7.157    172
       2859.50   7.156    171
       1155.27   2.891    116
       1149.05   2.876    240
       1142.58   2.859    139
       1093.75   2.737    129
       1087.65   2.722    234
       1081.18   2.706    125
        900.15   2.253   1000
        761.84   1.907     47
        758.54   1.899     45
        755.74   1.892    102
        752.69   1.884     91
        752.20   1.883    100
        750.49   1.878    151
        748.41   1.873     68
        746.70   1.869    107
        746.09   1.867     98
        744.38   1.863    177
        740.23   1.853     56
        737.92   1.847     75
        735.72   1.841     36
        726.93   1.819     35
        724.49   1.813     79
        722.53   1.808     64
        718.26   1.798    183
        716.43   1.793    110
        712.16   1.782    161
        711.18   1.780     92
        709.96   1.777     99
        707.28   1.770    110
        703.98   1.762     47
        701.17   1.755     42
        700.44   1.753     35
    

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    1H NMR 89.56 MHz
    C10 H13 N 0.04 ml : 0.5 ml CDCl3
    3-methyl-5,6,7,8-tetrahydroquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.170 B 7.142 C 2.87 D 2.71 E 2.244 F 1.90 to 1.74 400MHZ : HSP-40-251

         Hz     ppm     Int.
    

        732.50   8.179    169
        731.69   8.170    167
        730.88   8.161    171
        640.19   7.149    176
        639.63   7.142    174
        639.06   7.136    171
        262.69   2.934     86
        262.31   2.929     86
        262.00   2.926     85
        261.19   2.917     81
        257.13   2.872    190
        253.88   2.835     88
        253.50   2.831     87
        250.38   2.796    167
        246.63   2.754     83
        243.06   2.714    197
        238.13   2.659    127
        201.00   2.245   1000
        173.50   1.938     52
        173.13   1.934     50
        170.44   1.904    118
        168.75   1.885    126
        166.56   1.860    353
        163.81   1.830    286
        162.75   1.818    295
        159.88   1.786    341
        157.38   1.758    144
        155.63   1.738    114
        153.56   1.715     56
        153.19   1.711     55
    

in CDCl3

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liquid film

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