29815-94-9

双(4-氯苯氧基)乙酸(29815-94-9)核磁图(¹HNMR)

产品名称:双(4-氯苯氧基)乙酸

CAS:29815-94-9

分子式:C14H10Cl2O4

分子量: 313.13

Mass

MS-NW-8067          
bis(p-chlorophenoxy)acetic acid
C14H10Cl2O4         (Mass of molecular ion:    312)

   Source Temperature: 190 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      18.0       1.3
      28.0       1.5
      29.0       3.9
      36.0       1.1
      38.0       2.1
      39.0       4.3
      44.0       1.7
      45.0       1.2
      50.0       7.4
      51.0       5.6
      61.0       1.3
      62.0       1.7
      63.0       6.7
      64.0       3.9
      65.0      11.8
      66.0       1.3
      73.0       6.1
      74.0       3.1
      75.0      33.5
      76.0       7.1
      77.0       4.8
      85.0       2.9
      87.0       1.0
      93.0      16.0
      94.0       9.6
      99.0       8.8
     100.0       3.1
     101.0       3.5
     102.0       1.0
     111.0      56.5
     112.0       4.6
     113.0      19.1
     114.0       1.6
     127.0       4.7
     128.0     100.0
     129.0      32.0
     130.0      33.4
     131.0       9.9
     132.0       1.3
     139.0       4.6
     140.0       1.0
     141.0       4.5
     143.0       1.0
     150.0       1.5
     157.0       7.5
     159.0       2.5
     167.0      44.9
     168.0       5.5
     169.0      14.9
     170.0       1.5
     185.0      74.7
     186.0       7.4
     187.0      24.5
     188.0       2.4
     204.0       1.6
     267.0      10.0
     268.0       1.7
     269.0       6.4
     270.0       1.0
     271.0       1.1
     312.0      32.6
     313.0       5.1
     314.0      21.4
     315.0       3.3
     316.0       3.8

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₄ H₁₀ Cl₂ O₄	0.034 g : 0.5 ml DMSO-d₆
bis(p-chlorophenoxy)acetic acid

    Assign.     Shift(ppm)

      A             7.382
      B             7.099
      C             6.481

     Hz     ppm     Int.

   2958.98   7.404     71
   2955.57   7.396    811
   2953.13   7.390    268
   2951.17   7.385     43
   2950.68   7.384     43
   2948.73   7.379    274
   2946.29   7.373   1000
   2942.87   7.364    107
   2844.97   7.119     87
   2841.55   7.111    981
   2839.36   7.105    262
   2834.72   7.094    251
   2832.52   7.088    812
   2828.86   7.079     80
   2590.33   6.482    569

in DMSO-d6