52147-67-8

甲基亚磺酰基乙酸甲酯(52147-67-8)核磁图(¹HNMR)

产品名称:甲基亚磺酰基乙酸甲酯

CAS:52147-67-8

分子式:C4H8O3S

分子量: 136.17

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-8832          
methyl (methylsulfinyl)acetate
C4H8O3S             (Mass of molecular ion:    136)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      14.0       2.8
      15.0      24.0
      18.0       3.1
      27.0       3.7
      28.0       3.3
      29.0      11.4
      31.0       6.5
      33.0       1.8
      34.0       1.8
      35.0       2.1
      42.0      24.0
      43.0      37.9
      44.0       3.6
      45.0      21.8
      46.0       8.8
      47.0      10.6
      48.0       4.1
      49.0       1.7
      55.0       1.4
      57.0       1.6
      59.0      11.9
      61.0      10.2
      62.0       3.3
      63.0      64.8
      64.0       5.9
      65.0       3.1
      73.0      15.9
      74.0     100.0
      75.0       4.3
      77.0      12.2
      78.0       1.2
      79.0      30.3
      81.0       1.4
      89.0       2.5
      90.0       1.0
      91.0       3.5
      94.0       2.6
     104.0      11.3
     105.0      29.5
     106.0       2.1
     107.0       1.6
     119.0       1.1
     120.0       1.5
     121.0       1.8
     136.0      31.1
     137.0       5.5
     138.0       1.8

parameter in CDCl3

¹H NMR	300 MHz
C₄ H₈ O₃ S	0.05 ml : 0.5 ml CDCl₃
methyl (methylsulfinyl)acetate

    Parameter     ppm  Hz

      D(A)         3.801
     
      D(B)         3.759
     
      D(C)         2.754

     Hz     ppm     Int.

   1140.30   3.801   1000
   1127.71   3.759    472
    826.20   2.754    921

in CDCl3

liquid film

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甲基亚磺酰基乙酸甲酯(52147-67-8)核磁图(1HNMR)

甲基亚磺酰基乙酸甲酯(52147-67-8)核磁图(¹HNMR)