58885-58-8

N-(3-羟丙基)氨基甲酸叔丁酯(58885-58-8)核磁图(¹³CNMR)

产品名称:N-(3-羟丙基)氨基甲酸叔丁酯

CAS:58885-58-8

分子式:C8H17NO3

分子量: 175.23

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9209          
tert-butyl (3-hydroxypropyl)carbamate
C8H17NO3            (Mass of molecular ion:    175)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.4
      17.0       1.2
      18.0      10.9
      26.0       1.1
      27.0       6.1
      28.0      12.4
      29.0      18.0
      30.0      47.2
      31.0      10.9
      38.0       1.0
      39.0       9.7
      40.0       2.4
      41.0      43.8
      42.0       3.3
      43.0       7.2
      44.0      17.6
      45.0       2.1
      46.0       1.1
      53.0       1.3
      55.0       5.8
      56.0      18.2
      57.0     100.0
      58.0       9.6
      59.0      35.5
      60.0       1.2
      74.0       9.1
      75.0       4.4
      76.0      12.0
      84.0       2.4
      89.0       3.8
     101.0       4.4
     102.0       8.6
     116.0       1.2
     118.0       2.3
     119.0       9.3
     120.0       5.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₇ N O₃	0.05 ml : 0.5 ml CDCl₃
tert-butyl (3-hydroxypropyl)carbamate

    Assign.     Shift(ppm)

      A             5.27
      B             3.85
      C             3.651
      D             3.250
      E             1.678
      F             1.440

     Hz     ppm     Int.

   2105.22   5.268     31
   1546.02   3.869     27
   1540.53   3.855     52
   1534.79   3.841     33
   1467.65   3.673     53
   1462.04   3.659    114
   1456.30   3.644    107
   1450.56   3.630     41
   1310.18   3.279     38
   1304.08   3.264     90
   1297.85   3.248     92
   1291.63   3.232     43
    682.74   1.709     31
    676.88   1.694     82
    670.78   1.679    105
    664.67   1.664     74
    658.69   1.649     24
    575.44   1.440   1000

in CDCl3