80192-55-8

2,4-二乙基庚烷-1-醇(80192-55-8)核磁图(¹HNMR)

产品名称:2,4-二乙基庚烷-1-醇

CAS:80192-55-8

分子式:C11H24O

分子量: 172.31

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-0874          
2,4-diethyl-1-heptanol
C11H24O             (Mass of molecular ion:    172)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       4.9
      29.0       9.1
      31.0       3.8
      39.0       3.1
      41.0      24.8
      42.0       7.1
      43.0      70.4
      44.0       2.6
      45.0       1.8
      53.0       1.6
      54.0       1.1
      55.0      53.5
      56.0      17.1
      57.0      77.7
      58.0       3.7
      59.0       6.1
      67.0       2.5
      68.0       2.1
      69.0     100.0
      70.0      54.2
      71.0      36.4
      72.0       4.0
      73.0       3.8
      81.0       2.7
      82.0       1.5
      83.0      37.4
      84.0      25.1
      85.0      37.7
      86.0       3.3
      87.0       1.4
      95.0       2.2
      97.0       6.1
      98.0      62.6
      99.0      17.5
     100.0       1.2
     109.0       1.1
     110.0       2.8
     111.0      26.6
     112.0       6.5
     123.0       1.5
     124.0       2.5
     125.0      22.7
     126.0       3.3
     129.0       3.4
     139.0       2.0
     140.0       1.0
     141.0       1.6
     143.0       2.5
     154.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₂₄ O	0.05 ml : 0.5 ml CDCl₃
2,4-diethyl-1-heptanol

    Assign.     Shift(ppm)

      A     *1      3.531
      B     *1      3.494
      C             2.01
      D             1.47
      E             1.39
      F             1.29
      G     *2      1.23
      J     *2      1.15
      K     *3      0.894
      L     *3      0.885
      N             0.841

     Hz     ppm     Int.

   1422.85   3.561     60
   1420.65   3.555     59
   1417.97   3.549     64
   1415.65   3.543     61
   1412.23   3.534    172
   1410.03   3.529    198
   1407.35   3.522    171
   1405.03   3.516    198
   1402.95   3.511    195
   1401.00   3.506    163
   1397.09   3.496    183
   1395.26   3.492    156
   1392.33   3.484     64
   1390.38   3.479     65
   1386.47   3.470     58
   1384.52   3.465     66
    803.71   2.012    122
    601.68   1.506     40
    595.70   1.491     91
    589.72   1.476    127
    583.86   1.461    121
    578.13   1.447    104
    573.85   1.436     57
    572.14   1.432     63
    571.04   1.429     62
    567.75   1.421     58
    566.53   1.418     64
    564.82   1.414     99
    560.42   1.403    109
    558.59   1.398     78
    557.37   1.395     93
    554.08   1.387     82
    552.98   1.384    105
    551.27   1.380     84
    546.63   1.368     94
    544.43   1.363    101
    542.36   1.358     52
    540.65   1.353     98
    538.70   1.348    108
    537.11   1.344    119
    534.91   1.339    140
    533.45   1.335    143
    531.13   1.329    172
    529.66   1.326    185
    527.59   1.321    246
    523.56   1.311    338
    521.73   1.306    305
    519.78   1.301    300
    517.94   1.296    319
    516.48   1.293    361
    511.35   1.280    333
    508.30   1.272    255
    505.00   1.264    227
    501.95   1.256    167
    500.61   1.253    134
    497.92   1.246    128
    493.65   1.236    210
    487.79   1.221    233
    484.62   1.213     99
    481.69   1.206    156
    477.66   1.196     85
    474.85   1.189    143
    472.29   1.182     63
    468.14   1.172    190
    467.16   1.169    213
    460.69   1.153    292
    454.59   1.138    181
    448.12   1.122     77
    441.04   1.104     46
    364.99   0.914    549
    360.23   0.902    398
    357.67   0.895   1000
    356.93   0.894    990
    354.37   0.887    667
    353.27   0.884    646
    349.73   0.876    479
    347.05   0.869    386
    346.07   0.866    385
    343.26   0.859    496
    336.43   0.842    709
    335.82   0.841    695
    328.86   0.823    333

in CDCl3